Method of utilizing aqueous-organic chemical wastes from the fischertropsch process
阅读：165发布：2022-12-31
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1. A PROCESS FOR THE PRODUCTION OF LIQUID HYDROCARBONS AND OXYGENATED ORGANIC COMPOUNDS FROM CARBONACEOUS MATERIALS INVOLVING MAXIMUM UTILIZATION OF ACID-CONTAMINATED WASTE WATERS PRODUCED IN THE PROCESS, COMPRISING THE STEPS OF CONVERTING A CARBONACEOUS MATERIAL TO A SYNTHESIS GAS COMPRISING A MIXTURE OF HYDROGEN AND CARBON MONOXIDE BY REACTION OF SAID MATERIAL WITH STEAM AT ELEVATED TEMPERATURES IN A FIRST REACTION ZONE, PASSING SAID SYNTHESIS GAS TO A SECOND REACTION ZONE WHERE SAID GAS IS REACTED IN THE PRESENCE OF A CATALYST TO PRODUCE A PRODUCT COMPRISING A NONAQUEOUS PORTION INCLUDING LIQUID HYDROCARBONS AND OXYGENATED ORGANIC COMPOUNDS NORMALLY INSOLUBLE IN WATER, AND AN AQUEOUS PORTION CONTAINING DISSOLVED, WATER-SOLUBLE, OXYGENATED ORGANIC COMPOUNDS INCLUDING RELATIVELY LOW BOILING WATER SOLUBLE OXYGENATES CONSISTING CHIEFLY OF ALCOHOLS, ALDEHYDES, AND KETONES, AND LIKEWISE INCLUDING RELATIVELY HIGH BOILING, WATER SOLUBLE OXYGENATES CONSISTING CHIEFLY OF ORGANIC ACIDS, SEPARATING SAID NONAQUEOUS PORTION FROM SAID AQUEOUS PORTION, SEPARATING SAID RELATIVELY LOW BOILING, WATER SOLUBLE OXYGENATES FROM SAID AQUEOUS PORTION THEREBY LEAVING A DILUTE AQUEOUS SOLUTION CONTAINING THE BULK OF THE HIGHER BOILING WATER SOLUBLE OXYGENATES, INCLUDING SUBSTANTIALLY ALL THE ORGANIC ACIDS ORIGINALLY PRESENT IN SAID AQUEOUS PORTION, AND THEN PASSING THIS DILUTE ACID-CONTAINING SOLUTION TO SAID FIRST REACTION ZONE, WHEREBY THE WATER AND THE CARBON VALUES CONTAINED IN SAID ACID-CONTAMINATED SOLUTION ARE EMPLOYED FOR THE PRODUCTION OF SYNTHESIS GAS FOR SAID SECOND REACTION ZONE, THEREBY MAKING EFFECTIVE UTILIZATION OF AN OTHERWISE WASTE PRODUCT OF HIGHLY CORROSIVE PROPERTIES, AND AT THE SAME TIME ELIMINATING DISPOSAL PROBLEMS CONNECTED THEREWITH.
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