子分类：
| 序号 | 专利名 | 申请号 | 申请日 | 公开（公告）号 | 公开（公告）日 | 发明人 |
|---|---|---|---|---|---|---|
| 1 | 共沸干燥的卤化镍(II)的用途 | CN200480032160.9 | 2004-10-28 | CN1875027A | 2006-12-06 | G·哈德莱因; R·褒曼; M·巴尔奇; T·容坎普; H·鲁肯; J·沙伊德尔; H·舍费尔; W·塞格尔 |
| 本发明涉及一种制备含有至少一个镍(0)中心原子和至少一种磷配体的镍(0)－磷配体配合物的方法，该方法包括在至少一种磷配体存在下将通过共沸蒸馏干燥的卤化镍(II)还原。 | ||||||
| 2 | 共沸干燥的卤化镍(II)的用途 | CN200480032160.9 | 2004-10-28 | CN1875027B | 2011-11-09 | G·哈德莱因; R·褒曼; M·巴尔奇; T·容坎普; H·鲁肯; J·沙伊德尔; H·舍费尔; W·塞格尔 |
| 本发明涉及一种制备含有至少一个镍(0)中心原子和至少一种磷配体的镍(0)-磷配体配合物的方法，该方法包括在至少一种磷配体存在下将通过共沸蒸馏干燥的卤化镍(II)还原。 | ||||||
| 3 | JPS60501508A - | JP50220484 | 1984-05-25 | JPS60501508A | 1985-09-12 | |
| 4 | Telescoped multiwall nanotube and manufacture thereof | US11080010 | 2005-03-14 | US07238425B2 | 2007-07-03 | John P. Cumings; Alex K. Zettl; Steven G. Louie; Marvin L. Cohen |
| The invention relates to a method for forming a telescoped multiwall nanotube. Such a telescoped multiwall nanotube may find use as a linear or rotational bearing in microelectromechanical systems or may find use as a constant force nanospring. In the method of the invention, a multiwall nanotube is affixed to a solid, conducting substrate at one end. The tip of the free end of the multiwall nanotube is then removed, revealing the intact end of the inner wall. A nanomanipulator is then attached to the intact end, and the intact, core segments of the multiwall nanotube are partially extracted, thereby telescoping out a segment of nanotube. | ||||||
| 5 | Use of azeotropically dried nickel(ii) halogenides | US10577130 | 2004-10-28 | US20070073071A1 | 2007-03-29 | Gerd Haderlein; Robert Baumann; Michael Bartsch; Tim Jungkamp; Hermann Luyken; Jens Scheidel; Heinz Schafer; Wolfgang Siegel |
| A process is described for preparing a nickel(0)-phosphorus ligand complex containing at least one nickel(0)central atom and at least one phosphorus ligand, which comprises reducing a nickel(II) halide dried by azeotropic distillation in the presence of at least one phosphorus ligand. | ||||||
| 6 | (NF.sub.4).sub.2 NiF.sub.6 High energy solid propellant oxidizer and method of producing the same | US732623 | 1976-10-15 | US4108965A | 1978-08-22 | Karl O. Christe |
| The combination of the strongly oxidizing NF.sub.4.sup.+ cation with the strongly oxidizing NiF.sub.6.sup.-- anion in the form of the stable salt (NF.sub.4).sub.2 NiF.sub.6 produces a powerful oxidizer, useful for solid propellant formulations and NF.sub.3 -F.sub.2 gas generators. A process for its production is described. | ||||||
| 7 | Production of nickel fluoride | US12155471 | 1971-03-05 | US3836634A | 1974-09-17 | SALDICK J |
| A HIGHLY ACTIVE, ANHYDROUS NICKEL FLUORIDE WHICH IS RESISTANT TO PICK-UP OF ATMOSPHERIC WATER AND IS SUPERIOR AS A BATTERY ELEMENT IN HIGH ENERGY LITHIUM-NICKEL FLUORIDE BATTERIES, IS PRODUCED BY PASSING ANHYDROUS GASEOUS HYDROGEN FLUORIDE OVER AMORPHOUS BASIC NICKEL CARBONATE AT A TETEMPERATURE OF BETWEEN 150*-300*C. AND PREFERABLY 225*-250*C.
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| 8 | Method for forming metal fluoride material | US14221957 | 2014-03-21 | US09446966B2 | 2016-09-20 | Jon Shan |
| The present invention is directed to processing techniques and systems of metal fluoride based material, including but not limited to nickel difluoride, copper difluoride, manganese fluoride, chromium fluoride, bismuth fluoride, iron trifluoride, iron difluoride, iron oxyfluoride, metal doped iron fluorides, e.g., FexM1-xFy (M=metals, which can be Co, Ni, Cu, Cr, Mn, Bi and Ti) materials. An exemplary implementation involves mixing a first compound comprising a metal material, nitrogen, and oxygen to a second compound comprising hydrogen fluoride. The mixed compound is milled to form metal fluoride precursor and a certain byproduct. The byproduct is removed, and the metal fluoride precursor is treated to form iron trifluoride product. There are other embodiments as well. | ||||||
| 9 | Use of azeotropically dried nickel(ii) halogenides | US10577130 | 2004-10-28 | US07700795B2 | 2010-04-20 | Gerd Haderlein; Robert Baumann; Michael Bartsch; Tim Jungkamp; Hermann Luyken; Jens Scheidel; Heinz Schafer; Wolfgang Siegel |
| A process is described for preparing a nickel(0)-phosphorus ligand complex containing at least one nickel(0)central atom and at least one phosphorus ligand, which comprises reducing a nickel(II) halide dried by azeotropic distillation in the presence of at least one phosphorus ligand. | ||||||
| 10 | Process for the extraction of specific transition metals with gaseous HCL | US11166061 | 2005-06-24 | US07604784B2 | 2009-10-20 | Joseph L. Thomas |
| A process is disclosed for separation and recovery of vanadium, molybdenum, iron, tungsten, cobalt and nickel from alumina-based materials, mattes, ores, manufacturing by-products and waste. These elements are oxidized. The oxides are reacted with gaseous HCl to form volatile chloride-bearing compounds that subsequently sublimate. The volatile compounds are condensed in a downward-stepped thermal gradient that allows collection of moderate to high purity compounds of individual elements with exception of a nickel-cobalt co-condensate. Nickel is separated from cobalt by precipitation of nickel chloride from concentrated HCl pressurized with gaseous HCl. | ||||||
| 11 | Process for the extraction of specific transition metals with gaseous HCl | US11166061 | 2005-06-24 | US20090047198A1 | 2009-02-19 | Joseph L. Thomas |
| A process is disclosed for separation and recovery of vanadium, molybdenum, iron, tungsten, cobalt and nickel from alumina-based materials, mattes, ores, manufacturing by-products and waste. These elements are oxidized. The oxides are reacted with gaseous HCl to form volatile chloride-bearing compounds that subsequently sublimate. The volatile compounds are condensed in a downward-stepped thermal gradient that allows collection of moderate to high purity compounds of individual elements with exception of a nickel-cobalt co-condensate. Nickel is separated from cobalt by precipitation of nickel chloride from concentrated HCl pressurized with gaseous HCl. | ||||||
| 12 | Telescoped multiwall nanotube and manufacture thereof | US09915196 | 2001-07-24 | US06874668B2 | 2005-04-05 | John P. Cumings; Alex K. Zettl; Steven G. Louie; Marvin L. Cohen |
| The invention relates to a method for forming a telescoped multiwall nanotube. Such a telescoped multiwall nanotube may find use as a linear or rotational bearing in microelectromechanical systems or may find use as a constant force nanospring. In the method of the invention, a multiwall nanotube is affixed to a solid, conducting substrate at one end. The tip of the free end of the multiwall nanotube is then removed, revealing the intact end of the inner wall. A nanomanipulator is then attached to the intact end, and the intact, core segments of the multiwall nanotube are partially extracted, thereby telescoping out a segment of nanotube. | ||||||
| 13 | Production of nickel fluoride | US3607013D | 1969-02-10 | US3607013A | 1971-09-21 | SALDICK JEROME |
| A highly active, anhydrous nickel fluoride which is resistant to pickup of atmospheric water and is superior as a battery element in high energy lithium-nickel fluoride batteries, is produced by passing anhydrous gaseous hydrogen fluoride over amorphous basic nickel carbonate at a temperature of between 150*-300* C. and preferably 225*-250* C.
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| 14 | Preparation of anhydrous inorganic metal halides and organic complexes thereof | US3471250D | 1967-04-18 | US3471250A | 1969-10-07 | LANGER HORST G |
| 15 | 金属カルコゲニド薄膜電極、その生産方法及び使用 | JP2016557189 | 2014-12-04 | JP2017503084A | 2017-01-26 | ミヒャエル ラブロウ，; アナ フィッシャー，; マシアス ドリエス，; トーマス シェデル−ニードリグ，; マルセル−フィリップ ルーケ， |
| 本発明は、金属カルコゲニド薄膜電極を生産するための方法に関する。上記方法は、(a) 非水性溶媒中で金属又は金属酸化物とハロゲン元素とを接触させて、上記溶液中でハロゲン化金属化合物を生産するステップと、(b) ステップ(a)由来の上記溶液と接触している電気伝導性基板又は半導体基板に負電圧を印加するステップと、(c) ステップ(b)の間及び/又は後に、上記基板とカルコゲン元素とを接触させて、金属カルコゲニド層を前記基板上に形成するステップとを有する。また、本発明は、上記方法によって製造することができる金属カルコゲニド薄膜電極と、(光)電気化学的水分解の間、酸素を放出するアノードとしてのその使用に関する。【選択図】なし | ||||||
| 16 | Use of halogenated nickel was dried by azeotropic distillation (ii) | JP2006537183 | 2004-10-28 | JP2007509885A | 2007-04-19 | シェファー，ハインツ; シャイデル，イェンス; ズィーゲル，ヴォルフガング; ハーデルライン，ゲルト; バウマン，ローベルト; バルチュ，ミヒャエル; ユングカムプ，ティム; ルイケン，ヘルマン |
| 【課題】温和な条件でニッケル（０）錯体を製造することができ、熱的に不安定な配位子を使用することができ、過剰量の出発物質を使用する必要がないニッケル（０）錯体の製造方法を提供する。
【解決手段】本発明は、少なくとも１個のニッケル（０）中心原子と少なくとも１個のリン配位子とを含むニッケル（０）−リン配位子錯体の製造方法であって、少なくとも１種のリン配位子の存在下での共沸蒸留により乾燥させたハロゲン化ニッケル（ＩＩ）を還元する工程を含む方法である。 【選択図】なし |
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| 17 | PROCESS FOR THE EXTRACTION OF SPECIFIC TRANSITION METALS | EP06785032 | 2006-06-16 | EP1899271A4 | 2011-03-16 | THOMAS JOSEPH L |
| 18 | EXTRACTION OF METALS FROM ORES | EP84901943.0 | 1984-05-25 | EP0145728A1 | 1985-06-26 | LLOYD, Robert; TURNER, Maxwell, James |
| Les métaux sont extraits à partir de minerais qui existent sous la forme d'oxyde ou de sulfure, en traitant le minerai avec de l'acide fluorhydrique et/ou de l'acide fluorosilicique. Il existe deux formes préférées d'extraction. Lorsque l'on utilise de l'acide fluorhydrique, le minerai est d'abord broyé, séché puis mis au contact de gaz HF à des températures supérieures à 105oC pour produire des fluorures métalliques. Les fluorures métalliques sont ensuite mis au contact d'une solution aqueuse de HF (acide fluorhydrique) et les fluorures métalliques insolubles et les oxydes de fer obtenus sont séparés de la solution, et les fluorures métalliques de préférence y compris les fluorures de nickel et de cobalt sont récupérés. Lorsque l'on utilise de l'acide fluorosilicique, le minerai broyé et séché est mis en contact direct avec une solution aqueuse d'acide fluorosilicique à des températures supérieures à 70oC et les fluorures métalliques insolubles et les oxydes de fer obtenus sont séparés, et les fluorures métalliques, y compris de préférence les fluorures de nickel et de cobalt, sont récupérés. Les minerais préférés sont les minerais de cobalt-nickel latéritiques. | ||||||
| 19 | METALLCHALKOGENID-DÜNNSCHICHTELEKTRODE, VERFAHREN ZU IHRER HERSTELLUNG UND VERWENDUNG | EP14820763.2 | 2014-12-04 | EP3077332A1 | 2016-10-12 | LUBLOW, Michael; FISCHER, Anna; DRIESS, Matthias; SCHEDEL-NIEDRIG, Thomas; LÜCKE, Marcel-Philip |
| The invention relates to a method for producing a metal chalcogenide thin layer electrode, comprising the steps: (a) bringing a metal or metal oxide into contact with an elementary halogen in a non-aqueous solvent, generating a metal halogenide bond in the solution, (b) connecting a negative electrical voltage to an electrically conductive or semiconductive substrate which is in contact to the solution from step (a), and (c) during and/or after step (b), bringing the substrate into contact with an elementary chalcogen, forming a metal chalcogenide layer on the substrate. The invention furthermore relates to a metal chalcogenide thin layer electrode which can be produced by the method and use thereof as an anode for oxygen release in (photo)electrochemical water-splitting. | ||||||
| 20 | PROCESS FOR THE EXTRACTION OF SPECIFIC TRANSITION METALS | EP06785032.1 | 2006-06-16 | EP1899271B1 | 2012-08-01 | THOMAS, Joseph, L., |
| A process is disclosed for separation and recovery of vanadium, molybdenum, iron, tungsten, cobalt and nickel from alumina-based materials, mattes, ores, manufacturing by-products and waste. These elements are oxidized. The oxides are reacted with gaseous HCI to form volatile chloride- bearing compounds that subsequently sublimate. The volatile compounds are condensed in a downward-stepped thermal gradient that allows collection of moderate to high purity compounds of individual elements with exception of a nickel-cobalt co-condensate. Nickel is separated from cobalt by precipitation of nickel chloride from concentrated HCI pressurized with gaseous HCI. | ||||||
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