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Preparation of 1,1'-dimethyl-4,4'-bipyridylium dichloride

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专利汇可以提供Preparation of 1,1'-dimethyl-4,4'-bipyridylium dichloride专利检索,专利查询,专利分析的服务。并且PURPOSE: To prepare the titled compound useful as a non-selective herbicide, in high yield, by reacting 4, 4'-bipyridyl with mono-chloroacetic acid in the presence of water using a suspending agent compriing a phosphoric acid salt and if necessary an aminopolycarboxylic acid.
CONSTITUTION: The objective compound can be prepared without producing precipitate, by reacting 4, 4'-bipyridyl with monochloroacetic acid in the presence of water using a suspending agent comprising an alkali metal salt of phosphoric acid or its mixture with an aminopolycarboxylic acid and/or its salt, at 90W 130°C for 1W7hr. The obtained compound can be compound as it is with various adjuvants for herbicide. The phosphoric acid salt is primary W tertiary phosphate, pyrophosphate, polyphosphate and its K salt, Na salt, etc., and the aminopolycarboxylic acid is e.g. nitrilotriacetic acid, ethylenediaminetetraacetic acid, and its Na, K, ammonium salt, etc.
COPYRIGHT: (C)1984,JPO&Japio,下面是Preparation of 1,1'-dimethyl-4,4'-bipyridylium dichloride专利的具体信息内容。

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