| 序号 | 专利名 | 申请号 | 申请日 | 公开（公告）号 | 公开（公告）日 | 发明人 |
|---|---|---|---|---|---|---|
| 41 | Process for precipitating metal-containing compounds as gel-particles dispersed in aqueous phase | US17099471 | 1971-08-11 | US3826755A | 1974-07-30 | MC KENNA N; GRIMES J; SCOTT K |
| TO A SALT SOLUTION OR HYDROUS SOL OF THE METAL OR METALS IS ADDED A POLYMER WHICH IS EITHER A POLYSACCHARIDE HAVING A MAIN CHAIN OF 1-6 LINKAGES, OR OF 1-4 LINKAGES WITH SUBSTITUENT GROUPS HAVING ETHER OR ESTER LINKAGES, E.G. GUAR GUM, OR A POLYALCOHOL, E.G. POLYVINYL ALCOHOL, WHICH COMPLEXES WITH THE METAL IONS PRESENT. A PRECIPITATING REAGENT, E.G. AN ALKALINE SOLUTION, IS ADDED GRADUALLY TO THW VISCOUS MIXTURE THUS FORMED WHILE AGITATING THE MIXTURE, RESULTING IN THE FORMATION OF A GEL-PARTICULATE PRECIPITATE.
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| 42 | Removal of sulphur in recovery of nickel | US47606343 | 1943-02-16 | US2408311A | 1946-09-24 | HILLS ROBERT C; DUFOUR MAURICE F |
| 43 | Process for separating nickel and cobalt in solutions | US39567141 | 1941-05-28 | US2290313A | 1942-07-21 | CARON MARTINUS H |
| 44 | Impurity Containing Cathode Material with Preferred Morphology and Method to Prepare from Impurity Containing Metal Carbonate | US15517273 | 2015-09-30 | US20170309909A1 | 2017-10-26 | Jens PAULSEN; HeonPyo HONG; JinDoo OH |
| A carbonate precursor compound for manufacturing a lithium metal (M)-oxide powder usable as an active positive electrode material in lithium-ion batteries, M comprising 20 to 90 mol % Ni, 10 to 70 mol % Mn and 10 to 40 mol % Co, the precursor further comprising a sodium and sulfur impurity, wherein the sodium to sulfur molar ratio (Na/S) is 0.4 | ||||||
| 45 | Nickel metal compositions and nickel complexes derived from basic nickel carbonates | US12968341 | 2010-12-15 | US09371343B2 | 2016-06-21 | John J. Ostermaier |
| Nickel-metal-containing solids for use in manufacturing nickel metal complexes are disclosed. The nickel-metal-containing solids are made by reducing basic nickel carbonates. By varying the molar ratios of carbonates and bicarbonates to nickel salts, the methods provide basic nickel carbonates that produce superior nickel metal-containing solids that react more effectively with phosphorous-containing ligands. The phosphorous containing ligands can be both monodentate and bidentate phosphorous-containing ligands. | ||||||
| 46 | METHOD FOR PRODUCING SIZE SELECTED PARTICLES | US14265638 | 2014-04-30 | US20140341797A1 | 2014-11-20 | Gregory K. Krumdick; Young Ho Shin; Kaname Takeya |
| The invention provides a system for preparing specific sized particles, the system comprising a continuous stir tank reactor adapted to receive reactants; a centrifugal dispenser positioned downstream from the reactor and in fluid communication with the reactor; a particle separator positioned downstream of the dispenser; and a solution stream return conduit positioned between the separator and the reactor. Also provided is a method for preparing specific sized particles, the method comprising introducing reagent into a continuous stir reaction tank and allowing the reagents to react to produce product liquor containing particles; contacting the liquor particles with a centrifugal force for a time sufficient to generate particles of a predetermined size and morphology; and returning unused reagents and particles of a non-predetermined size to the tank. | ||||||
| 47 | Nickel compositions for preparing nickel metal and nickel complexes | US12968373 | 2010-12-15 | US08815186B2 | 2014-08-26 | John J. Ostermaier |
| Nickel compositions for use in manufacturing nickel metal compositions, and specifically to methods of making basic nickel carbonates used to produce nickel metal compositions are disclosed. By varying the molar ratios of carbonates and bicarbonates to nickel salts, the methods provide basic nickel carbonates that produce superior nickel-containing solids that react more effectively with phosphorous-containing ligands. The phosphorous containing ligands can be both monodentate and bidentate phosphorous-containing ligands. | ||||||
| 48 | Process for production of nickel carbonate | US13430362 | 2012-03-26 | US08747795B2 | 2014-06-10 | Tiago Valentim Berni; Antonio Clareti Pereira; Felipe Hilario Guimar{hacek over (a)}es |
| Aspects of the present invention refers to a process for production of nickel carbonate including preparing a magnesium salt solution, contacting the solution with a stream of gaseous CO2, keeping pH between 4 and 10 and temperature between 0 and 100° C., during up to 5 hours to produce a first mixture, contacting the first mixture with a nickel sulphate solution to produce a second mixture, performing a separation of liquid and solid portions of the second mixture, and feeding the magnesium salt solution with the liquid portion. This process recycles the reagent used for producing nickel carbonate and yields a final product that is easy to handle and transport. | ||||||
| 49 | COMPOSITE PRECURSOR, COMPOSITE PREPARED THEREFROM, METHOD OF PREPARING THE COMPOSITE, POSITIVE ELECTRODE FOR LITHIUM SECONDARY BATTERY INCLUDING THE COMPOSITE, AND LITHIUM SECONDARY BATTERY EMPLOYING THE POSITIVE ELECTRODE | US13837183 | 2013-03-15 | US20140057177A1 | 2014-02-27 | Jun-Seok Park; Yong-Chan You; Chang-Wook Kim; Jae-Hong Lim; Sang-Woo Cho; Ji-Hyun Kim |
| A composite precursor is represented by Formula 1, and includes primary particles having an average particle diameter of about 1 nm to about 10 nm. A composite is prepared from the composite precursor. A method of preparing the composite includes mixing the composite precursor with a lithium compound to obtain a mixture, and thermally treating the mixture to obtain the composite. A positive electrode for a lithium secondary battery includes the composite, and a lithium secondary battery includes the positive electrode. NiaMnbCocMd(CO3)2 Formula 1 | ||||||
| 50 | PROCESS FOR PRODUCTION OF NICKEL CARBONATE | US13430362 | 2012-03-26 | US20120269713A1 | 2012-10-25 | Tiago Valentim BERNI; Antonio Clareti Pereira; Felipe Hilário Guimarães |
| Aspects of the present invention refers to a process for production of nickel carbonate including preparing a magnesium salt solution, contacting the solution with a stream of gaseous CO2, keeping pH between 4 and 10 and temperature between 0 and 100° C., during up to 5 hours to produce a first mixture, contacting the first mixture with a nickel sulphate solution to produce a second mixture, performing a separation of liquid and solid portions of the second mixture, and feeding the magnesium salt solution with the liquid portion. This process recycles the reagent used for producing nickel carbonate and yields a final product that is easy to handle and transport. | ||||||
| 51 | Composite carbonate and method for producing the same | US13014855 | 2011-01-27 | US08066915B2 | 2011-11-29 | Yasuhiro Nakaoka |
| The present invention provides a method for producing a nickel atom-, manganese atom- and cobalt atom-containing composite carbonate that is high in specific surface area and large in tap density, and useful as a raw material for producing a lithium nickel manganese cobalt composite oxide to be used in a positive electrode active material for use in a lithium secondary battery. The composite carbonate includes nickel atoms, manganese atoms and cobalt atoms, and has an average particle size of 5 μm or more and less than 20 μm, a BET specific surface area of 40 to 80 m2/g and a tap density of 1.7 g/ml or more. | ||||||
| 52 | COMPOSITE CARBONATE AND METHOD FOR PRODUCING THE SAME | US12362918 | 2009-01-30 | US20090194746A1 | 2009-08-06 | Yasuhiro Nakaoka |
| The present invention provides a nickel atom-, manganese atom- and cobalt atom-containing composite carbonate that is high in specific surface area and large in tap density, and useful as a raw material for producing a lithium nickel manganese cobalt composite oxide to be used in a positive electrode active material for use in a lithium secondary battery, and provides a method for industrially advantageously producing the composite carbonate. The composite carbonate includes nickel atoms, manganese atoms and cobalt atoms, and has an average particle size of 5 μm or more and less than 20 μm, a BET specific surface area of 40 to 80 m2/g and a tap density of 1.7 g/ml or more. | ||||||
| 53 | Cobalt encapsulated nickel hydroxides and basic carbonates for battery electrodes | US10635906 | 2003-08-07 | US07267874B2 | 2007-09-11 | John Ernest Fittock; Cheryl Christine Lucas; Katherine Fiona Howison |
| A process for producing a cobalt III encapsulated nickel hydroxide or basic nickel carbonate product including the steps of: (i) providing an ammoniacal solution including cobalt ammine complexes and nickel II ammine complexes; (ii) progressively lowering the ammonia content to sequentially precipate the nickel as an hydroxide or basic carbonate; and (iii) further lowering the ammonia content to precipitate the majority of the cobalt as cobalt III oxide hydroxide; wherein the majority of cobalt III oxide hydroxide coats on the surface of the precipitate nickel hydroxide or basic nickel carbonate to form a coated particle. | ||||||
| 54 | Recovery of nickel and cobalt carbonates from ammoniacal leach solutions | US615801 | 1975-09-22 | US4002719A | 1977-01-11 | Utah Tsao |
| An ammonium carbonate leach solution containing dissolved nickel and/or cobalt values is sprayed into a flash chamber to flash a portion of the ammonia therefrom, resulting in the production of a fine precipitate of nickel and/or cobalt carbonate. The solution is introduced into a stripping tower wherein remaining ammonia is stripped therefrom to precipitate further nickel and/or cobalt carbonate on the previously precipitated carbonate, which function as nuclei to reduce deposition in the column. | ||||||
| 55 | Method for contact between fluids | US37626673 | 1973-07-03 | US3905900A | 1975-09-16 | GULYAS JAMES W; VYDRA CHARLES |
| Precipitation of solids from a liquid is effected in a confined contact zone by passing the liquid downwardly through a rising stream of hot gas. A number of light weight spheres are confined within and freely movable throughout the zone. The upper and lower limits of the zone are defined by partitions each composed of a horizontal foraminous divider and an imperforate wall. The imperforate wall extends upwardly and outwardly from the divider and terminates at a wall defining the side limit of the zone. The velocity of the rising gas is highest as it passes through the divider and decreases upwardly therefrom. The gas causes the spheres resting on the divider to move upwardly and outwardly until the gas velocity is no longer capable of keeping the spheres in suspension whereupon the spheres fall downwardly along the side wall and imperforate wall scouring solids precipitated thereon.
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| 56 | Removal of cobalt from nickel salt solutions | US39328673 | 1973-08-31 | US3903246A | 1975-09-02 | GANDON LOUIS; BOZEC CHRISTIAN; LENOBLE PHILIPPE |
| A compound for use as an oxidizing agent in an aqueous saline reaction medium, having a base of nickel salts which is a basic nickel III carbonate of the general formula:
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| 57 | Removal of cobalt from nickel salt solutions | US29037772 | 1972-09-19 | US3890243A | 1975-06-17 | GANDON LOUIS; BOZEC CHRISTIAN; LENOBLE PHILIPPE |
| A composition suitable for use as an oxidizing agent in an aqueous saline solution is disclosed comprising a major portion of a basic nickel III carbonate having the formula
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| 58 | Method of preparing hydrated nickel carbonate and the product thereof | US31168163 | 1963-09-26 | US3350167A | 1967-10-31 | MCMULLEN WARREN H; MOONEY THOMAS J; STODDARD JR WILLIAM B |
| 59 | Method of manufacturing nickel carbonate | JP2014500208 | 2012-03-26 | JP2014511813A | 2014-05-19 | ティアゴ、バレンティム、ベルニ; アントニオ、クラレティ、ペレイラ; フェリペ、イラリオ、ギマランイス |
| 本発明は、炭酸ニッケルの製造方法であって、ａ）マグネシウム塩溶液を用意する工程と、ｂ）前記溶液をＣＯ ２ガスの流れに接触させ、５時間以下の間、ｐＨを４〜１０に保持し、かつ、温度を０〜１００℃に保持する工程と、ｃ）工程ｂ）の混合物を硫酸ニッケル溶液と接触させて、混合物を生成する工程と、ｄ）前記混合物の液体部分および固体部分の分離を行う工程と、ｅ）前記液体部分を工程ａ）に供給する工程とを含む、方法に関するものである。 この方法によれば、炭酸ニッケルの製造に使用した試薬がリサイクルされ、取り扱いおよび輸送が容易な最終製品が得られる。 | ||||||
| 60 | Method for manufacturing aggregated particle of metal, method for manufacturing positive electrode active material for lithium ion battery, method for manufacturing lithium ion battery, and lithium ion battery | JP2012012417 | 2012-01-24 | JP2013151383A | 2013-08-08 | DOTANI AKIRA; GOTO HIDENORI |
| PROBLEM TO BE SOLVED: To obtain aggregated particles of metal having stable particle diameters and to obtain substantially spherical aggregated particles of metal.SOLUTION: A method for manufacturing aggregated particles of metal has a circulation mechanism in which the flow of a metal-containing liquid passes through a treatment vessel 10 and external circulation paths 20, 22, 26, 28 and part of the liquid in the treatment vessel 10 is substantially continuously extracted from the extraction outlet 20 to the outside, passed through the suction side path 22 and the discharge side path 26 of the external circulation paths, and returned to the treatment vessel 10 through the return path 28. A flow rate in the external circulation paths 20, 22, 26, 28 is ≥1 m/s and a stock solution A or a stock solution B containing at least part of reactants to be newly added is poured into the external circulation paths 22, 26. | ||||||
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