序号 专利名 申请号 申请日 公开(公告)号 公开(公告)日 发明人
1 一种节能型金属钠盐及其制备方法和应用 CN201610617948.0 2016-07-29 CN106241836A 2016-12-21 陈虎; 李娜; 徐培; 迟韵; 刘娟
发明属于工业盐的生产领域,特别涉及一种节能型金属钠盐及其制备方法和应用。将普通金属钠盐过筛去除大颗粒盐和粉盐,再与氟化钠、醋酸钠等助剂按照一定的质量比例混匀,混匀后得到新型金属钠盐。本发明制备的新型金属钠盐,SO42-含量低于0.02%,该产品作为工业生产金属钠的专用原料盐,能够将制备金属钠的三元体系和二元体系的共融温度降低5-20℃,电导提高1-5%,且工艺简单,操作方便,对产品和环境无污染,成本低,适合大规模工业化生产。
2 一种光照下能够释放负离子的氯化钠盐砖制备方法 CN201710165522.0 2017-03-20 CN106904640A 2017-06-30 张继森; 段维江; 徐增山
一种光照下能够释放负离子的氯化钠盐砖制备方法,该方法包括以下步骤:步骤一,把原料盐放入高温炉中,3h内加热到5000℃,然后在2~3h内降温到3000℃,再自然降温到室温,获得了预处理产品A;步骤二,把预处理产品A研磨30min后过80目筛,收集过筛后粉末并装入模具内,在40MPa下保持10min,脱模后获得预处理产品B;步骤三,把预处理产品B重新移入高温炉中并在10min内加热到3000℃并保温1h后继续在1h内升温到7000℃,再在4h内降温到5000℃后迅速升温到8000℃,然后在2h内再降温到7000℃;步骤四,把步骤三中去除分和吸附气体的预处理产品B从7000℃迅速升温到11000℃并保持3h后,再在6~8h内降温到室温,即可获得最终产品。该盐砖可用于室内装饰和汗蒸保健。
3 一种采用硫化染料滤液制备硫代硫酸氯化钠的方法 CN201610150810.4 2016-03-17 CN105819407A 2016-08-03 王嘉兴
一种采用硫化染料滤液制备硫代硫酸氯化钠的方法,它涉及染料化学工业三废综合治理和利用的技术领域,它的制备方法为:将硫化染料的化滤液与盐酸稀溶液反应器中进行反应,生成硫代硫酸和氯化钠混合溶液,将混合溶液进行过滤,滤液送进减压蒸馏器里进行减压蒸馏,然后冷却结晶,洗涤,干燥得到了氯化钠晶体产品,剩余的蒸馏液体放置在净化器内,然后放入氢氧化形成氯化银沉淀,过滤后剩余的氢氧化钠溶液再加入氯化进行中和得到氢氧化钙沉淀,再进行过滤,减压蒸馏、浓缩最后得到硫代硫酸液体。它方法简单,将废弃的氧化滤液重新利用,制得硫代硫酸和氯化钠产物,能有效的治理和利用了硫化染料氧化滤液,保护了环境,节约了资源。
4 低堆积密度空心金属化合物细粉的生产方法 CN95115215.7 1995-08-03 CN1127676A 1996-07-31 窪谷笃芳; 石桥修; 小野功一
一种低堆积密度空心的金属化合物细粉可通过一步法由该化合物的溶液生产。按照本发明生产碱金属化合物的低堆积密度空心细粉的方法包括碱金属化合物的水溶液与脉动燃烧气体接触的步骤。
5 Method for producing a low bulk density fine particles of the alkali metal compound JP20031894 1994-08-03 JP3650422B2 2005-05-18 功一 小野; 修 石橋; 篤芳 窪谷
6 Apparatus for controlling crystal particle diameter of product JP28685293 1993-11-16 JPH07138017A 1995-05-30 SHINDO TOSHIHARU; ISHIMARU NAOYUKI; NINOMIYA NAOYOSHI; HASEGAWA MASAMI
PURPOSE:To stably control the particle diameter of product crystal by preventing the oscillation and non-linearity of the crystallization phenomenon in a salt-forming process. CONSTITUTION:The characteristics of a crystallizing apparatus (a) exhibiting oscillation property and nonlinearity in a crystallization system 20 of a salt- forming process are modeled by a model-constructing function part 11 using a learning function of a neural net based on a measurement data on product crystal particle diameter having distribution. The crystallization factors to get target values are inferred from the target product crystal particle diameter based on the constructed model. In the case of varying operation state, the crystallization operation conditions for getting the target average crystal particle diameter are inferred on the crystallization factors other than the factors to cause the variation of the operation state. The inference is carried out by judging the effective range based on the maximum value, the representative mean value and the minimum value of the product crystal particle diameter.
7 Plant for producing pressure die-cast or injection moulded articles using salt cores EP98119334.5 1998-10-13 EP0909600A1 1999-04-21 Moschini, Renzo

Plant (1) for producing pressure die-cast or injection moulded articles having a unit (2) for producing salt grains (10), a press (3) for forming salt filler cores by compressing the said salt grains (10), a pressure die-casting machine (4) for making the said articles by injecting a material in the liquid state into a mould having at least one salt filler core, and a salt removal and washing unit (5) designed to remove the salt filler cores that have been trapped within the said articles; the said unit (2) for producing salt grains (10) being designed to atomize a saline solution which is supersaturated with salt into a plurality of drops so as subsequently to cause the salt present in solution/suspension in each drop of solution to solidify into a corresponding salt grain (10).

8 Method for the preparation of pellets of metal halide EP93116467.7 1993-10-12 EP0592998A1 1994-04-20 Wataya, Kazuhiro; Sakai, Shigeru; Fukuda, Masahiko; Yoshida Norifumi

An improvement is obtained in the method for the preparation of pellets of a metal halide as a light-emitting source of metal halide lamps, of which an extremely low moisture content is essential, in order not to increase the moisture content of the metal halide during pulverization and compression molding of the metal halide. Thus, a metal halide dehumidified in advance to have a moisture content not exceeding 5 ppm is pulverized and compression-molded in an atmosphere of an inert gas of which the dew point is -60 °C or lower so that substantially no moisture absorption takes place during processing.

9 PROCESS FOR SYNTHESIZING A COMPACTED PRODUCT US12539688 2009-08-12 US20100040882A1 2010-02-18 Robin PHINNEY
A method forming a potassium chloride particle form potassium chloride powder having resistance to moisture absorption and shrinkage. The original feedstock comprises potassium chloride in a size distribution of 30 mesh and 100 mesh as well as a gluten based binder.
10 Method for producing pressure die-cast or injection moulded articles using salt cores US09169970 1998-10-13 US06458297B2 2002-10-01 Renzo Moschini
Method for producing pressure die-cast or injection moulded articles having a unit for producing salt grains, a press for forming salt filler cores by compressing the said salt grains, a pressure die-casting machine for making the said articles by injecting a material in the liquid state into a mould having at least one salt filler core, and a salt removal and washing unit designed to remove the salt filler cores that have been trapped within the said articles; the said unit for producing salt grains being designed to atomize a saline solution which is supersaturated with salt into a plurality of drops so as subsequently to cause the salt present in solution/suspension in each drop of solution to solidify into a corresponding salt grain.
11 Use of dodecylbenzene sulfonic acid or salt as a scale inhibitor US09676259 2000-09-28 US06436154B1 2002-08-20 Aileen M. Halverson; Duane S. Halverson
The formation of scale on equipment surface in contact with sodium alkali containing brines is inhibited by the addition of an alkylbenzene sulfonic acid or salt thereof to the brines.
12 Process for crystallization of mineral salts US688913 1996-07-31 US5716419A 1998-02-10 David A. Larsen
Mineral salts, e.g., potassium chloride, are crystallized from aqueous solutions thereof in the presence of a crystal growth promoting amount of lecithin or lecithin containing compositions. Mineral salts include alkali metal and alkaline-earth metal chloride, sulfate, carbonate, phosphate and nitrate salts. The process is described as providing increased amounts of large crystals and a narrower and more uniform crystal size distribution.
13 Compacts of spray dried water soluble compounds US233767 1988-08-19 US5108726A 1992-04-28 Roger A. Baldwin; Virgil J. Barczak
The present invention is directed to articles of manufacture comprising solid compacts, formed at elevated pressures, from homogenous, finely divided powders of spray dried water soluble inorganic compounds. The solid compacts are characterized by their readily water dissolvable, substantially nondusting and dense nature.
14 Stabilization of solid sodium chloride against mushing in an aqueous medium US339965 1989-04-18 US4992208A 1991-02-12 Donald T. Ireland
A method and composition are described for the prevention of the mushing or the disintegration of solid sodium chloride in an aqueous medium.
15 Process for the production of salt US940220 1986-12-08 US4797981A 1989-01-17 Leon Ninane; Claude Breton
Process for the production of salt in which sodium chloride is crystallized in the form of spheres by evaporation of a sodium chloride brine and the spheres obtained are then broken up. The salt produced by the process is particularly suitable for the food industry.
16 Potash granulation US3711254D 1970-02-25 US3711254A 1973-01-16 CORMODE H; MC GOWAN J; KIRBY C
PARTICULATE POTASH IS GRANULATED IN A PAN GRANULATOR. THE MOIST GRANULES FROM THE PAN ARE MIXED WITH WARM RECYCLED DRY GRANULES AND TUMBLED IN A ROTATING DRUM WHEREBY THE GRANULES BECOME EQUILIBRATED IN BOTH MOISTURE CONTENT AND TEMPERATURE. THE EQUILIBRATED GRANULES ARE DRIED IN A FLUID BED DRYER AND SIZED BY SCREENING. THE OVERSIZE AND UNDERSIZE GRANULES ARE RECYCLED, VIA A PULVERIZER, TO THE PAN AND THE PRODUCT SIZE GRANULES GO TO STORAGE. THE RECYCLED DRY GRANULES ARE EITHER TAKEN FROM THE DRYER DISCHARGE OR FROM THE PRODUCT SIZE GRANULES GOING TO STORAGE. THE FINAL PRODUCT IS A GRANULATED POTASH OF IMPROVED BULK DENSITY, HARDNESS AND GRANULE SHAPE WHICH IS SUITABLE FOR USE IN BULK BLEND FERTILIZERS.
17 Sodium chloride crystals US3567371D 1967-07-28 US3567371A 1971-03-02 BIRCHALL JAMES DEREK
PREPARATION OF A NOVEL CRYSTAL FORM OF SODIUM CHLORIDE BY EVAPORATING SODIUM CHLORIDE BRINES CONTAINING CERTAIN ADDITIVES. THE NOVEL CRYSTAL FORM COMPRISES A CUBE HAVING RECTILINEAR COLUMNS OF RECTANGULAR, USUALLY SQUARE SECTION ATTACHED PERPENDICULARLY TO AT LEAST ONE PAIR OF ADJACENT FACES OF THE CUBES. TO THE COLUMNS THEMSELVES CAN ALSO BE ATTACHED, PERPENDICULARLY, FURTHER RECTILINEAR COLUMNS, AND SO ON, AND THE PERPENDICULAR POSITIONING HOLDS THE CRYSTALS APART FROM ONE ANOTHER IN THE MASS AND THE BULK-DENSITY OF SUCH A MASS IS CONSEQUENTLY LOW. THE ADDITIVES INCLUDE POLYVINYL ALCOHOL EITHER ALONE OR IN ASSOCIATION WITH POLYELECTROLYTES THAT GIVE RISE TO POLY-

ANIONS, AND COMBINATIONS OF A WATER-SOLUBLE POLYELECTROLYTE AND SALTS ABLE TO YIELD INORGANIC IONS THAT FORM INSOLUBLE OR SPARINGLY SOLUBLE SALTS WITH THE POLYIONS OF THE POLYELECTROLYTE. PARTICULARLY EFFECTIVE IS 1 TO 100 PARTS BY WEIGHT PER MILLION OF BRINE OF POLY(VINY ALCOHOL) OF MOLECULAR WEIGHT SUCH THAT THE VISCOSITY OF A 1% BY WEIGHT AQUEOUS SOLUTION AT 20*C. IS 1.1 TO 1.6 CENTISTOKES; OR A COMBINATION OF 5 TO 50 PARTS OF SODIUM ALGINATE AND 250-500 PARTS OF CALCIUM IONS BY WEIGHT PER MILLION OF BRINE.
18 Process and apparatus for harvesting crystals US46291465 1965-06-10 US3389974A 1968-06-25 CESARE BARATTINI; PAOLO BORTOLINI; ALBERTO SCARFI
1,099,318. Crystallizing. SOCIETA' EDISON. June 9, 1965 [June 10, 1964], No. 24466/ 65. Heading B1G. [Also in Division F4] Cooling and crystallization of a saturated solution is effected in a vessel by means of water-cooled heat exchange tubing 1 resiliently suspended from a frame 2 which is vibrated by a cam operated by a motor 18. The tubing is in the form of two bundles operating in parallel, each bundle comprising a plurality of tubes, each connected to the next alternately at the top and bottom. The solution is stirred by a propellor 19 between the bundles.
19 Crystallizing under vacuum US18607062 1962-04-09 US3195990A 1965-07-20 WITTE JOHAN F
In order to avoid foaming during crystallisation of a solution of urea, the solution is first freed from gases by reduction of pressure at a temperature above the crystallization temperature of the solution.
20 Manufacture of meat curing salt US75188734 1934-11-07 US2054625A 1936-09-15 GRIFFITH ENOCH L
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