Crystallizing under vacuum |
|||||||
申请号 | US18607062 | 申请日 | 1962-04-09 | 公开(公告)号 | US3195990A | 公开(公告)日 | 1965-07-20 |
申请人 | WERKSPOOR NV; | 发明人 | WITTE JOHAN F; | ||||
摘要 | In order to avoid foaming during crystallisation of a solution of urea, the solution is first freed from gases by reduction of pressure at a temperature above the crystallization temperature of the solution. | ||||||
权利要求 | 1. A PROCESS FOR CRYSTALLIZING SOLUTIONS DEVELOPING GASES WHEN SUBJECTED TO A VACUUM, SAID PROCESS COMPRISING THE STEPS OF CONTINUOUSLY FEEDING A SOLUTION THROUGH A PREEVAPORATOR TO A CRYSTALLIZER IN BOTH OF WHICH A VACUUM IS MAINTAINED, CONTINUOUSLY WITHDRAWING THE CRYSTAL SLURRY FORMED INTHE CRYSTALLIZER, PASSING A PORTION OF THE CRYSTAL SLURRY TO A CLASSIFIER TO SEPARATE SAID SLURRY INTO FINE AND COARSE FRACTIONS, SUPPLYING A PORTION OF THE COARSE FRACTION TO THE PRE-EVAPORATOR, AND MIXING THE COARSE FRACTION WITH THE SOLUTION TO BE CRYSTALLIZED IN THE PRE-EVAPORATOR WHILE MAINTAINING THE ABSOLUTE PRESSURE IN THE PREEVAPORAATOR GREATER THAN THAT IN THE CRYSTALLIZER TO AN EXTENT THAT NO CRYSTALLIZATION OF THE SOLUTION TAKES PLACE IN THE PRE-EVAPORATOR. |
||||||
说明书全文 |