首页 / 专利分类库 / 有机化学 / 无环或碳环化合物 / 有羧基连接六元芳环碳原子上的化合物
序号 专利名 申请号 申请日 公开(公告)号 公开(公告)日 发明人
101 리신 P-이소부틸 페닐프로피온산 유도체의 제조방법 KR1019770001238 1977-05-26 KR1019810001025B1 1981-08-31 알버토레이너
Title compd. (I) was prepd. by reacting lysine salt derived from lysine derivs. with p-isobutylphenylpropionic acid. I was water sol. and had higher antirheumatic and analgetic activity than 2-(p-isobutylphenyl)propionic acid. Thus, I was more effective than the acid in suppressing inflammation in rats due to injection of kaolin. The acute i.p. LD50 of I was 149.7 mg/kg in mice and 485.3 in rats.
102 分離芳基羧酸之方法 TW102110995 2013-03-27 TW201343622A 2013-11-01 阿督里 帕凡庫瑪; ADURI, PAVANKUMAR; 尤帕拉 帕拉蘇 維拉; UPPARA, PARASU VEERA; 簡恩 蘇瑞許 香堤爾; JAIN, SURESH SHANTILAL; 瑞納帕其 尤戴; RATNAPARKHI, UDAY
本發明提供一種將芳基羧酸從包含多個芳基羧酸之混合物中分離出來的方法,其中,該方法包括加熱含有至少兩個芳基羧酸的第一混合物,其中每個該芳基羧酸均有其預定的液化溫度和預定的沈澱溫度,在預定溫度下,通過至少一個離子化合物得到液化組合物;溫控條件下冷卻液化成分以分級結晶並沈澱一個芳基羧酸。分離沈澱之芳基羧酸,將得到的母液反復冷卻直至逐個沈澱每個剩餘芳基羧酸。母液仍保持液態。
103 純對苯二甲酸化母液的處理設備 TW106216798 2017-11-10 TWM563292U 2018-07-11 陳麗崑; CHEN, LI KUN; 俞國平; YU, KUO PING; 陳明裕; CHEN, MING YU
The present invention provides an acid water and residue separation device for a mother liquor discharged from an oxidation unit of pure terephthalic acid (PTA), comprising a precipitation tank; a precision filtration tank; and an auxiliary crystallization device, wherein the mother liquid is A mother liquid tank flows out into the precipitation tank and crystallizes and precipitates solid particles therein, and then flows out into the precipitation tank to enter the precision filter tank for filtration, and a part of the filtered clarified mother liquid flows back to the mother liquid tank, and another part flows into the auxiliary tank. The crystallization apparatus adjusts the conditions of the clarified mother liquid, returns to the precipitation tank, and circulates the above-mentioned filtration to obtain a clarified mother liquid. The solid residue adhering to the precision filtration tank is discharged from the bottom of the precision filtration tank through a cake program after the filtration is stopped, and collected and then subjected to cobalt manganese recovery treatment. The creation can improve the high energy consumption and high power consumption of the vaporized acid water in the traditional process, and can also reduce the loss of cobalt and manganese bromine catalyst caused by the mother liquor discharge, thereby achieving the purpose of energy saving and consumption reduction.
104 방향족 카르복시산 제조방법 KR1020120134974 2012-11-27 KR101467635B1 2014-12-01 이윤우; 김대성; 최성환; 최광호
알킬방향족화합물의부분산화반응을통한방향족카르복시산제조방법에있어서, 특정첨가제를이용하여초임계이산화탄소에대한기존촉매의용해도를향상시켜특별한비용의추가부담없이방향족카르복시산의수율을향상시키는방법이개시된다. 본발명은알킬방향족화합물의부분산화반응을통한방향족카르복시산제조방법에있어서, (a) 반응기에알킬방향족화합물및 반응촉매를도입하는단계; (b) 상기반응기에기체상의용매및 산화제를도입하는단계; (c) 상기반응기에상기알킬방향족화합물의부분산화반응을증가시키기위한반응촉진제를도입하는단계; (d) 상기반응기내부의온도및 압력을증가시켜상기기체상의용매를초임계유체상으로형성되도록하여, 상기초임계유체상에상기알킬방향족화합물, 상기반응촉매, 상기산화제및 상기반응촉진제가모두용해되어, 상기반응기내부가단일상의상태로되어부분산화반응이진행되도록하는단계; 및 (e) 상기반응기내부를감압하여상기기체상의용매를제거하는단계;를포함하는것을특징으로하는방향족카르복시산제조방법을제공한다.
105 순수 형태를 포함하는 방향족 카르복실산의 제조 방법 및제조 장치 KR1020077024038 2006-03-20 KR101432517B1 2014-08-22 바토스토마스엠; 렁라이너스케이
방향족 카르복실산의 제조를 위한 방법 및 장치는, 방향족 탄화수소 공급 재료의 액상 산화, 및 물과 반응 용매를 분리하고 또 분리로부터 얻어지는 가스 및 액체 상들 사이에 액상 산화 부산물 종 (species) 을 우선적으로 배분하기 위한 액상 산화로부터 나온 고압 오프가스의 처리를 포함한다. 순수 형태의 방향족 카르복실산의 제조 방법이 또한 포함된다. 방향족 카르복실산, 제조 방법 및 제조 장치.
106 아로마틱폴리카본산의 제조방법 KR1019980057387 1998-12-22 KR1020000041506A 2000-07-15 정성화; 박윤석
PURPOSE: An efficient method for the preparation of an aromatic polycarbonic acid is provided which prevents reduction of reaction activity in the latter part of the reaction, reduces side reactions, and chromaticity of the aromatic polycarbonic acid prepared therefrom is excellent. CONSTITUTION: A method for the preparation of the aromatic polycarbonic acid comprises carrying out oxidation reaction of polyalkylaromatic compound or its oxidized intermediates dissolved in an aliphatic carbonic acid having 1 - 6 carbon atom, in the presence of a catalyst system comprising cobalt, manganese and bromine, with a gas containing highly concentrated oxygen to prepare the aromatic polycarbonic acid, characterized by further adding at least one transition metal or lanthanide metal component to the catalyst system in order to prevent lowering of reaction activity in the latter part of the reaction due to use of the gas containing highly concentrated oxygen.
107 아로마틱폴리카본산의제조방법 KR1019980057386 1998-12-22 KR1020000041505A 2000-07-15 정성화; 박윤석
PURPOSE: An efficient method for the preparation of an aromatic polycarbonic acid is provided which improves reaction activity and reduces side reactions. CONSTITUTION: A method for the preparation of the aromatic polycarbonic acid comprises carrying out oxidation reaction of polyalkylaromatic compound or its oxidized intermediates dissolved in an aliphatic carbonic acid having 1 - 6 carbon atom, in the presence of a catalyst system comprising cobalt, manganese and bromine, with an oxygen-containing gas to prepare the aromatic polycarbonic acid, characterized by further adding at least one alkali metal or alkali earth metal component to the catalyst system.
108 메칠-3,4-디하이드록시-5-메톡시 벤조레이트의 제조방법 KR1019910025394 1991-12-30 KR1019950005767B1 1995-05-30 김승조
The preparation method for methyl 3,4-dihydroxy-5-methoxy benzolate (I) consists of reacting gallic acid with 4-6M dimethyl sulfate as alkylating agent and 4-6M sodium carbonate or potassium carbonate, borate as protectant for 3,4-hydroxy group in water, acetone or acetonitrile, methanol or ethanol (4:10:5) to prevent pH change. (I) is useful as intermediate for biphenyl carbonate.
109 광학적 활성 알파-아릴알카노산의 제조방법 KR1019850002311 1985-04-06 KR100059440B1 1993-02-16 클라우디오기오르다오; 그라지아노카스탈디; 풀비오우게리; 실비아카비치올리
110 나프탈렌으로부터 실질적으로 나프토퀴논을 함유하지 않는 프탈산 무수물을 제조하는 방법 KR1019920009658 1992-06-04 KR1019930000461A 1993-01-15 만프레드츄어하우젠; 칼키르스테; 빌프리드크릭스
내용 없음
111 2,4-디클로로-5-플루오로-벤조산의 제조방법 KR1019850006988 1985-09-24 KR100054446B1 1992-09-07 프리츠마우러; 클라우스고르에
112 2,4,5-트리할로게노- 및 2,3,4,5-테트라할로게노벤젠 유도체의 제조방법 KR1019850003889 1985-06-04 KR1019920005845B1 1992-07-23 에리히클라우케; 우베페터슨; 클라우스그로에
내용 없음.
113 2,4-디클로로-5-플루오로-벤조산의 제조방법 KR1019850006988 1985-09-24 KR1019910008936B1 1991-10-26 프리츠마우러; 클라우스고르에
내용 없음.
114 술폰아미드기를 함유하는 페녹시벤조산 유도체의 제조방법 KR1019820003344 1982-07-27 KR100027651B1 1989-03-16 엘-아마디아이헤이바
115 술폰아미드기를 함유하는 페녹시벤조산 유도체의 제조방법 KR1019820003344 1982-07-27 KR1019880002591B1 1988-12-03 엘-아마디아이헤이바
Phenoxy benzoic sulphonamides of formula (I) and their salts [R=CON(R4) SO2R3; A=H, halogen, N=NCF3, PO3H2 and its alkyl esters, NHCOR, NH2, etc.; B=H, halogen, alkyl, alkoxy, NHCOR, NH2, etc.; C=H, halogen, alkyl, alkylamino; D=halogen, CF3, alkylthio, haloalkyl, etc.; E=H, haloalkyl, alkoxy, alkylsulphinyl, CN, CF3, NHCOR1, NH2, etc.; F=B; R1=alkyl, alkoxy, mono or dialkylamino; R2=alkyl, phenyl; R3=phenyl, pyridyl, NO, alkenyl, alkynyl, substd. alkyl, etc.; R4=H, alkyl were prepd. by reaction in the presence of an acid acceptor of an acid halide (II)(R=COX; X=Cl, Br, I) with a sulphonamide, R3SO2NH. Thus, 5-[2'-chloro-4'(trifluoromethyl)-phenoxy -2- nitrobenzoyechloride was treated with MeSO2NH2 to give 71% (I) (R=NHSO2Me, A=NO2, B=Cl, D=CF3, C,E,F=H).
116 2,4-디클로로-5-플루오로-벤조산의 제조방법 KR1019850006988 1985-09-24 KR1019860002446A 1986-04-26 프리츠마우러; 클라우스고르에
내용 없음
117 술폰아미드기를 함유하는 페녹시벤조산 유도체의 제조방법 KR1019820003344 1982-07-27 KR1019840000466A 1984-02-22 엘-아마디아이헤이바
내용없음
118 직접 중합 반응에 사용 되는 테레프탈산의 제조 방법 KR1019820000716 1982-02-18 KR1019830008974A 1983-12-16 시게야쓰모또-8
내용없음
119 PRODUCTION OF AROMATIC ACIDS AND PHENOLICS PCT/NL2020/050654 2020-10-22 WO2021080426A1 2021-04-29 CROCKATT, Marc

The invention is directed to a process for the preparation of an aromatic acid or a phenolic compound, said process comprising reacting a dienophile and a furanic compound comprising an acetal moiety in a Diels-Alders reaction to obtain an aromatic compound comprising said acetal moiety, followed by hydrolysis and oxidation of said acetal moiety into a hydroxide or carboxylate moiety to form the aromatic acid or phenolic compound, wherein said dienophile is selected from the group consisting of alkylenes, acetylenes, acrylates, maleates, fumarates, maleimides, propiolates, acetylene dicarboxylates, and benzynes and wherein said acetal moiety is bound directly to the 2-position of the furanic compound.

120 이소프로필 알코올의 제조 방법 PCT/KR2013/005739 2013-06-28 WO2014003475A1 2014-01-03 이성규; 이종구; 신준호

본 출원은 이소프로필 알코올의 제조 방법에 관한 것이다. 본 출원에서는, 물과 이소프로필 알코올을 포함하는 피드로부터 이소프로필 알코올을 고순도로 수득할 수 있다. 또한, 이소프로필 알코올의 수득 과정에서 사용되는 에너지 및 제조 설비를 위한 투자비 등도 절감할 수 있다.

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