101 |
Alkyl sulfate/alkyl ether sulfate mixture and use |
JP18444888 |
1988-07-22 |
JPS6447756A |
1989-02-22 |
UBUE PUROOKU; BUORUFUGANGU HOOHOSHIYOON |
|
102 |
Sulfurized hydroxy ether, manufacture and use |
JP17796388 |
1988-07-15 |
JPS6438056A |
1989-02-08 |
GIRUBERUTO SHIENKAA; ROBERUTO PIOORU; ZABIINE RIYUTSUTOUGE |
|
103 |
Manufacture of sulfate betaine |
JP6067088 |
1988-03-16 |
JPS63243065A |
1988-10-07 |
GERORUDO BURAUN; CHIYUNNII CHIYAN; KURISUTOSU FUAMUFUAKARISU; KURAUSU GURAAZERU |
|
104 |
JPS6314707B2 - |
JP9542481 |
1981-06-22 |
JPS6314707B2 |
1988-04-01 |
KAARU JOOJI KURESUPAN |
|
105 |
Continuous sulfation method |
JP18045984 |
1984-08-31 |
JPS6160643A |
1986-03-28 |
HIRAKOUCHI YOSHIE; TAKAHASHI MASATOSHI |
PURPOSE: To carry out the continuous sulfation, and to obtain high-quality sulfated product in an industrial scale, suppressing the side reactions, by forming a fluid thin film of an organic compound by a high-speed gas stream formed along the wall surface, and contacting the film of the organic compound with chlorosulfonic acid.
CONSTITUTION: A high-speed gas stream flowing downward is formed along the inner wall of te reaction tube 11 from the high-speed gas inlet 17. A liquid organic compound (e.g. 8W20C straight or branched-chain alcohol) is supplied from te raw material inlet 19 along the inner wall, and is formed to a circular thin liquid film by the high-speed gas stream. Chlorosulfonic acid is introduced through the inlet 31, and sprayed by the inert gas, etc. introduced from the gas inlet 33. The sprayed chlorosulfonic acid is contacted with the organic compound to effect the continuous sulfation of the compound. Since the organic compound is reacted in the formula thin film, the heat-exchange efficiency is high, and since the chlorosulfonic acid is contacted and absorbed in the form of fine particles, it can be added uniformly to the organic compound, and a sulfated product containing little unreacted organic compound and by-product can be produced.
COPYRIGHT: (C)1986,JPO&Japio |
106 |
Sulfurization of compound containing hydroxyethyl group |
JP18380785 |
1985-08-21 |
JPS6157546A |
1986-03-24 |
HANSURUDORUFU SHIYUBUANDAA |
|
107 |
JPS6012347B2 - |
JP5161275 |
1975-04-30 |
JPS6012347B2 |
1985-04-01 |
RAASUROO FUOIAA; AARUPAADO FURUKA; FUERENTSU SHEBESHUTEIEEN; YOORAN HERUCHERU; ERUJEEBETO BENDEIFUI |
1504541 Compositions containing amino acid derivatives CHINOIN GYOGYSZER ES VEGYESZETI TERMEKEK GYARA RT 28 April 1975 [29 April 1974 26 March 1975] 17608/75 Heading A5B [Also in Divisions C2 and C3] Cosmetic and pharmaceutical compositions contain (I) and/or salts thereof as active ingredient wherein A<SP>1</SP> stands for hydroxy, C 1-4 alkoxy, cycloalkoxy, aralkoxy, substituted aralkoxy, aryloxy, substituted aryloxy or a group of the general formulae: wherein R<SP>14</SP> is hydrogen, C 1-4 alkyl or aralkyl, R<SP>6</SP> is hydrogen, C 1-5 alkyl, aralkyl, hydroxysubstituted aralkyl, heteroaralkyl or a group of the general formula: Y is hydroxy, amino, alkylamino, dialkylamino, C 1-4 alkoxy or aralkoxy, and r is an integer of from 1 to 10 or an average polymerization grade of up to 2000, B<SP>1</SP> is a group of the formulae -SO 2 OH, -OSO 2 OH, -O-PO(OH) 2 or -S-S-R<SP>11</SP>, wherein R<SP>11</SP> is C 1-4 alkyl, aralkyl or aryl or a residue obtained when removing group B<SP>1</SP> from the general formula (I), R stands for hydrogen, C 1-4 alkyl or aralkyl, R<SP>x</SP> stands for hydrogen or halogen, R<SP>1</SP> stands for hydrogen, C 1-4 alkyl, aryl, aryl having a nitro or alkoxy substituent, aralkyl, substituted aralkyl, alkoxycarbonyl, cycloalkoxycarbonyl, aralkoxycarbonyl, substituted aralkoxycarbonyl having, e.g. a halogen, alkoxy, nitro, phenylazo or alkoxyphenylazo substituent, unsubstituted or substituted aryloxycarbonyl, acyl, arylsulfonyl or group (wherein R<SP>6</SP> has the same meanings as defined above and p is an integer of from 1 to 10 or an average polymerization degree of up to 2000), R<SP>2</SP> stands for hydrogen, C 1-4 alkyl, or aralkyl or R<SP>2</SP> and R<SP>2</SP> may each stand for a -CO- group and form a ring through an o-phenylene, alkylene or -CH=CH- group, R<SP>3</SP> stands for hydrogen, carboxy or carbalkoxy, R<SP>4</SP> stands for hydrogen, halogen, C 1-4 alkyl or hydroxy, R<SP>5</SP> stands for hydrogen, halogen, C 1-4 alkyl, carboxy, carboxamido, carbalkoxy or carboaralkoxy, m is 1, 2 or 3, n is 1, 2, 3 or 4, s is 0, 1, 2, 3 or 4, and t is 1, 2 or 3. |
108 |
JPS5951937B2 - |
JP6205877 |
1977-05-27 |
JPS5951937B2 |
1984-12-17 |
BAATON BURUTSUKUSU; RICHAADO JEI BURUTSUKUSU |
|
109 |
JPS5943936B2 - |
JP14406677 |
1977-12-02 |
JPS5943936B2 |
1984-10-25 |
KAARU JOOJI KURESUPAN |
|
110 |
Copolymer |
JP20472382 |
1982-11-24 |
JPS5891708A |
1983-05-31 |
KAARU JIYOOJI KURESUPAN |
|
111 |
Omega-fluorosulfato-perfluoro-(2-methyl- alkane-3-one) and manufacture of perfluoro- isopropylketocarboxylic acid fluoride derived therefrom |
JP14255381 |
1981-09-11 |
JPS5781455A |
1982-05-21 |
HANSU MIRAUERU; GIYUNTERU JIIGEMUNTO; UERUNERU SHIYUUERUTOFUEGERU |
|
112 |
Manufacture of polyfluorocarbonyl compounds and some novel compounds among these compounds |
JP14255281 |
1981-09-11 |
JPS5781434A |
1982-05-21 |
HANSU MIRAUERU; GIYUNTERU JIIGEMUNTO; UERUNERU SHIYUUERUTOFUEGERU |
|
113 |
Preparation of perfluorocarbonyl sulfonic acid fluoride |
JP14255581 |
1981-09-11 |
JPS5779186A |
1982-05-18 |
HANSU MIRAUERU; UERUNERU SHIYUUERUTOFUEGERU |
|
114 |
N-allenylalkyl-acetanilides, manufacture and fungicidal composition |
JP11236881 |
1981-07-20 |
JPS5756445A |
1982-04-05 |
BUINFURIITO RUNKENHAIMAA; BUORUFUGANGU HIYUURAA; IERUKU SHIYUTETSUTAA; BUIRUHERUMU BURANDESU |
|
115 |
JPS5715113B2 - |
JP11518277 |
1977-09-27 |
JPS5715113B2 |
1982-03-29 |
|
|
116 |
Biodegradable zwitterionic surfactant compound and detergent composition containing it |
JP854281 |
1981-01-22 |
JPS56150048A |
1981-11-20 |
JIYOOJI EDOWAADO UENTORAA; JIYOSEFU MAKUGURADEII; YUUJIN POORU GOSERINKU; UIRIAMU AJIARON SHIRII |
|
117 |
Natural resin acid surfactant compound and surfactant made therefrom |
JP11745279 |
1979-09-14 |
JPS5540690A |
1980-03-22 |
URURITSUHI KUNTSUTSUE; HAINTSU UURITSUHI |
|
118 |
JPS5417591B2 - |
JP11909076 |
1976-10-04 |
JPS5417591B2 |
1979-06-30 |
|
|
119 |
Purification of sulfuric ester slats of higher alcohols or ethylene oxide adducts thereof |
JP12905377 |
1977-10-26 |
JPS5463021A |
1979-05-21 |
YOSHIDA SEIICHI; YAMASHITA NOBORU; YAMADA MINORU; YAMAGAMI MITSURU |
PURPOSE: To obtain highly pure title compound quite easily, which is an anionic surface active agent. by purifying the crude compound in the presence of H
2O
2.
CONSTITUTION: Highly pure sulfuric ester salt of a higher alcohol such as 12W13C oxo alcohol, or ehylene oxide adduct thereof, is obtained by purifying the crude compound in the presence of 0.001W1%, preferably 0.002W0.05%, based on the sulfuric ester salt of higher alcohol or the ethylene oxide adduct thereof, of H
2O
2, a peroxy acid or their salts, and reacting at 10W100°C for 20W180 min.
EFFECT: IMproved stability against the use of perfumes or dyes.
USE: Base of household detergents, shampoo, etc.
COPYRIGHT: (C)1979,JPO&Japio |
120 |
Preparation of alcohol sulfuric acid ester salt |
JP11518277 |
1977-09-27 |
JPS5452031A |
1979-04-24 |
YAMAGUCHI HACHIROU |
PURPOSE: To prepare an almost colorless title compound in high yield with little side ractions under mild conditions, by sulfating a primary or secondary alcohol having 6-18 C atoms using a complex of boric anhydride and sulfur trioxide as novel sulfating agent.
CONSTITUTION: An alcohol sulfuric acid ester salt (e.g. cyclohexanol sulfuric acid ester ammonium salt) is prepared by sulfating a 6-18C primary or secondary alcohol (e.g. cyclohexanol) in a solvent pref. comprising dimethylformamide containing a chlorinated alkane such as 1,2-dichloroethane, at a low temperature (e.g. -20- -10°C) using a complex of boric anhydride and sulfur trioxide obtained by the reaction of boric anhydride with sulfur trioxide in a solvent, as sulfating agent
COPYRIGHT: (C)1979,JPO&Japio |