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Process for the evaporation of volatile alcohols and sulphur in the course of black liquor evaporation

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专利汇可以提供Process for the evaporation of volatile alcohols and sulphur in the course of black liquor evaporation专利检索,专利查询,专利分析的服务。并且A process is provided for reducing the emission of volatile alcohols and sulphur compounds during the evaporation of black liquor in several effects in the sulphate cellulose process. The liquor in those effects which are working with the most diluted liquor is evaporated in two or more steps on the same pressure level. The liquor is carried through the steps in series, the vapours obtained from these steps are condensed and at least a part of the condensates obtained are reintroduced into the process or purified by means of distillation.,下面是Process for the evaporation of volatile alcohols and sulphur in the course of black liquor evaporation专利的具体信息内容。

1. A process for reducing the emission of volatile alcohols and sulphur compounds in the evaporation of black liquor in multiple effects in the sulphate cellulose process and in which at least those effects working with the most diluted liquor themselves comprise several serially connected steps, comprising preevaporating the liquor in those effects which are working with the most diluted liquor in two or more steps at the same pressure level, carrying the liquor through the steps in series, condensing the vapours obtained from these steps and reintroducing at least a part of the condensates thus obtained into the process.
2. The process of claim 1, in which the liquor of at least two subsequent evaporation effects of higher concentration is evaporated in two or more steps in each effect.
3. The process of claim 1, in which at least 30 percent, of the evaporation vapour from those effects which work with the most diluted liquor is condensed in a first methanol-poor fraction and the rest in a second methanol-enriched fraction, which fractions are reintroduced into the process or purified by distillation.
4. The process of claim 1, in which the final evaporation of the most concentrated liquor is carried out in parallel with liquor received from an intermediate evaporation effect following pre-evaporation.
5. The process of claim 1, in which the vapours after condensation are supplied to a distillation column which is working with reflux and that the heat content of the vapours leaving the distillation column is recovered in the process.
6. The process of claim 5, in which the pressure in the top of the distillation column is kept at from 0.5 to 4 atm.
7. The process of claim 5, in which the reflux to the distillation column is obtained by bringing the vapour leaving the column to condense partially in indirect heat exchange with liquor in a liquor evaporator, in which the evaporation is carried out at a lower pressure than the pressure prevailing in the distillation column, and in which evaporator uncondensed vapor resulting from the incomplete condensation and containing volatile alcohols and sulphur compounds after pressure-reduction is discharged to destruction or recovery and from which evaporator the condensed liquid phase obtained in said incomplete condensation in the liquor evaporator is returned to the distillation column.
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