| 序号 | 专利名 | 申请号 | 申请日 | 公开（公告）号 | 公开（公告）日 | 发明人 |
|---|---|---|---|---|---|---|
| 61 | SODIUM ANTI-PEROVSKITE SOLID ELECTROLYTE COMPOSITIONS | EP14900270 | 2014-08-22 | EP3192118A4 | 2018-02-21 | ZHAO YUSHENG; WANG YONGGANG; ZOU RUQIANG |
| Na-rich electrolyte compositions provided herein can be used in a variety of devices, such as sodium ionic batteries, capacitors and other electrochemical devices. Na-rich electrolyte compositions provided herein can have a chemical formula of Na3OX, Na3SX, Na (3-δ) Mδ/2OX and Na (3-δ) Mδ/2SX wherein 0<δ<0.8, wherein X is a monovalent anion selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof, and wherein M is a divalent metal selected from the group consisting of magnesium, calcium, barium, strontium and mixtures thereof. Na-rich electrolyte compositions provided herein can have a chemical formula of Na (3-δ) Mδ/3OX and/or Na (3-δ) Mδ/3SX; wherein 0<δ<0.5, wherein M is a trivalent cation M3, and wherein X is selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof. Synthesis and processing methods of NaRAP compositions for battery, capacitor, and other electrochemical applications are also provided. | ||||||
| 62 | COMPLEXOMETRIC PRECURSOR FORMULATION METHODOLOGY FOR INDUSTRIAL PRODUCTION OF HIGH PERFORMANCE FINE AND ULTRAFINE POWDERS AND NANOPOWDERS FOR SPECIALIZED APPLICATIONS | EP14767613.4 | 2014-03-14 | EP3245682A2 | 2017-11-22 | FRIANEZA-KULLBERG, Teresita |
| A method of forming a powder MjXp wherein Mj is a positive ion or several positive ions selected from alkali metal, alkaline earth metal or transition metal; and Xp is a monoatomic or a polyatomic anion selected from Groups IIIA, IVA, VA, VIA or VIIA; called complexometric precursor formulation or CPF. The method includes the steps of: providing a first reactor vessel with a first gas diffuser and an first agitator; providing a second reactor vessel with a second gas diffuser and a second agitator; charging the first reactor vessel with a first solution comprising a first salt of Mj; introducing gas into the first solution through the first gas diffuser, charging the second reactor vessel with a second solution comprising a salt of Mp; adding the second solution to the first solution to form a complexcelle; drying the complexcelle, to obtain a dry powder; and calcining the dried powder of said MjXp. | ||||||
| 63 | METHOD FOR PRODUCING MELT-CAST POTASSIUM FLUORINE-PHLOGOPITE | EP15875778.1 | 2015-10-28 | EP3241816A1 | 2017-11-08 | GUSEV, Alexandr Olegovich; SIMAKOV, Dmitriy Aleksandrovich; SLUCHENKOV, Oleg Valentinovich |
The invention relates to the preparation of synthetic melted mica materials, and specifically relates to a stone casting process and to the composition of an initial feedstock, and may be used in the creation of novel types of stone casting in the metallurgical, mining/enrichment, refractory and construction industries. A method for producing melt-cast potassium fluorine-phlogopite includes preparing feedstock by mixing mica-containing and fluorine-containing components, melting the produced feedstock, pouring the melt into a mold, allowing to sit, removing the casting from the mold, and cooling; according to the claimed invention, the mica-containing component consists of vermiculite (60-90 wt% and the fluorine-containing component consists of potassium cryolite 10-40wt%, wherein, the feedstock is melted via the sequential stepped heating thereof, and the feedstock is prepared by layering components, wherein the top layer of the feedstock consists of a mixture of components, and the melt is poured into a preheated mold. The use of the present invention allows for enhancing the chemical purity of the potassium fluorine-phlogopite, increasing the corrosion and erosion resistance of the material, and improving the accuracy of the chemical composition of the yielded product. |
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| 64 | SODIUM ANTI-PEROVSKITE SOLID ELECTROLYTE COMPOSITIONS | EP14900270.1 | 2014-08-22 | EP3192118A1 | 2017-07-19 | ZHAO, Yusheng; WANG, Yonggang; ZOU, Ruqiang |
| Na-rich electrolyte compositions provided herein can be used in a variety of devices, such as sodium ionic batteries, capacitors and other electrochemical devices. Na-rich electrolyte compositions provided herein can have a chemical formula of Na3OX, Na3SX, Na (3-δ) Mδ/2OX and Na (3-δ) Mδ/2SX wherein 0<δ<0.8, wherein X is a monovalent anion selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof, and wherein M is a divalent metal selected from the group consisting of magnesium, calcium, barium, strontium and mixtures thereof. Na-rich electrolyte compositions provided herein can have a chemical formula of Na (3-δ) Mδ/3OX and/or Na (3-δ) Mδ/3SX; wherein 0<δ<0.5, wherein M is a trivalent cation M3, and wherein X is selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof. Synthesis and processing methods of NaRAP compositions for battery, capacitor, and other electrochemical applications are also provided. | ||||||
| 65 | FLUORINATING AGENT | EP14850310 | 2014-10-02 | EP3053875A4 | 2017-03-15 | HARA SHOJI; KISHIKAWA YOSUKE; SHIRAI ATSUSHI; NAMIKAWA TAKASHI; ISHIHARA SUMI |
| 66 | METHOD FOR PRODUCING HEXAFLUOROPHOSPHATE SALT | EP08704433 | 2008-02-05 | EP2123601A4 | 2012-04-04 | WAKI MASAHIDE; MIYAMOTO KAZUHIRO; AOKI KENJI |
| In the manufacturing method of hexafluorophosphate (MPF 6 : M = Li, Na, K, Rb, Cs, NH 4 , and Ag) of the present invention, at least a H x PO y F z aqueous solution, a hydrofluoric acid aqueous solution, and MF · r (HF) are used as raw materials (wherein, r ‰¥ 0, 0 ‰¤ x ‰¤ 3, 0 ‰¤ y ‰¤ 4, and 0 ‰¤ z ‰¤ 6). According to the above description, a manufacturing method of hexafluorophosphate can be provided which is capable of manufacturing hexafluorophosphate (GPF 6 : G = Li, Na, K, Rb, Cs, NH 4 , and Ag) at a low cost in which the raw materials can be easily obtained, the control of the reaction is possible, and the workability is excellent. | ||||||
| 67 | Stabilized thiocarbonate solutions and the use thereof for controlling soil pests | EP89306901.3 | 1989-07-06 | EP0366226B1 | 1994-09-14 | Young, Donald C.; Green II, James A. |
| 68 | TETRATHIOCARBONATE PROCESS | EP90915039.0 | 1990-10-01 | EP0494933A1 | 1992-07-22 | HATTER, Marjorie, M.; WONG, Charles, F. |
| On produit des sels d'acide tétrathiocarbonique selon un procédé consistant à faire réagir de manière séquentielle ou continue un hydroxyde (16), un sulfure d'hydrogène (22), du soufre (12) et du disulfure de carbone (18). Les sels produits se présentent sous la forme de solutions aqueuses ayant des concentrations d'environ 15 à environ 55 pour cent en poids. | ||||||
| 69 | Stabilized solid thiocarbonate compositions and methods for making same | EP89313039.3 | 1989-12-13 | EP0376550A2 | 1990-07-04 | Pilling, Richard L.; Young, Donald C. |
Particles of thiocarbonate salts, thioesters or complexes are stabilized by being isolated from contact with water, CO₂ and oxygen and are encapsulated in a coating effective to prevent future contact of the particles with water, CO₂ and oxygen. The particles are preferably prepared in an environment from which water, CO₂ and oxygen are excluded. The coating may be a wax, a water-free oil or grease, sulfur or a natural or synthetic polymerizable resin. Various preparative and encapsulating techniques are disclosed. |
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| 70 | Stabilized thiocarbonate solutions and the use thereof for controlling soil pests | EP89306901.3 | 1989-07-06 | EP0366226A1 | 1990-05-02 | Young, Donald C.; Green II, James A. |
Aqueous thiocarbonate solutions are stabilized by the addition of base, sulfide and/or polysulfide and the stability and safety of the more concentrated solutions containing 1 weight percent or more equivalent CS₂ as a thiocarbonate are achieved as reflected by significant reduction of CS₂ partial pressure in such solutions. Such stabilized thiocarbonate solutions are useful for the control of pests in, e.g. soil, and for inhibiting nitrification. |
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| 71 | METHOD OF PRODUCING NITRIDE FLUORESCENT MATERIAL | US15842133 | 2017-12-14 | US20180171221A1 | 2018-06-21 | Sadakazu WAKUI; Shigeki YOSHIDA; Shoji HOSOKAWA |
| Provided is a production method of a nitride fluorescent material capable of producing a nitride fluorescent material having a higher emission intensity. The production method is for producing a nitride fluorescent material having a composition containing at least one element Ma selected from the group consisting of Sr, Ca, Ba and Mg, at least one element Mb selected from the group consisting of Li, Na and K, at least one element Mc selected from the group consisting of Eu, Ce, Tb and Mn, and Al and N, which includes subjecting a raw material mixture containing elements constituting the composition of the nitride fluorescent material, along with SrF2 and/or LiF added thereto as a flux, to a heat treatment, wherein the amount of the flux is in a range of 5.0% by mass or more and 15% by mass or less relative to the total amount, 100% by mass of the raw material mixture and the flux. | ||||||
| 72 | METHOD FOR PRODUCING MELT-CAST POTASSIUM FLUORINEPHLOGOPITE | US15540534 | 2015-10-28 | US20180002186A1 | 2018-01-04 | Aleksandr Olegovich GUSEV; Dmitriy Aleksandrovich SIMAKOV; Oleg Valentinovich SLUCHENKOV |
| The invention relates to the preparation of synthetic melted mica materials, and specifically relates to a stone casting process and to the composition of an initial feedstock, and may be used in the creation of novel types of stone casting in the metallurgical, mining/enrichment, refractory and construction industries. A method for producing melt-cast potassium fluorine-phlogopite includes preparing feedstock by mixing mica-containing and fluorine-containing components, melting the produced feedstock, pouring the melt into a mold, allowing to sit, removing the casting from the mold, and cooling; according to the claimed invention, the mica-containing component consists of vermiculite (60-90 wt % and the fluorine-containing component consists of potassium cryolite 10-40 wt %, wherein, the feedstock is melted via the sequential stepped heating thereof, and the feedstock is prepared by layering components, wherein the top layer of the feedstock consists of a mixture of components, and the melt is poured into a preheated mold. The use of the present invention allows for enhancing the chemical purity of the potassium fluorine-phlogopite, increasing the corrosion and erosion resistance of the material, and improving the accuracy of the chemical composition of the yielded product. | ||||||
| 73 | NONAQUEOUS ELECTROLYTIC SOLUTION FOR ELECTRIC DOUBLE LAYER CAPACITORS | US15534234 | 2014-12-11 | US20170330700A1 | 2017-11-16 | Yoshihisa TOKUMARU; Yoshihiro OKADA; Taiji NAKAGAWA; Shoji HIKETA; Koichi SORAJO |
| The present invention provides a nonaqueous electrolytic solution that provides an electric double layer capacitor having excellent durability. The nonaqueous electrolytic solution of the present invention is a nonaqueous electrolytic solution for electric double layer capacitors prepared by dissolving a quaternary ammonium salt as an electrolyte in a nonaqueous solvent, and the nonaqueous electrolytic solution has an alkali metal cation concentration of 0.1 to 30 ppm. | ||||||
| 74 | SODIUM ANTI-PEROVSKITE SOLID ELECTROLYTE COMPOSITIONS | US15505890 | 2014-08-22 | US20170275172A1 | 2017-09-28 | Yusheng ZHAO; Yonggang WANG; Ruqiang ZOU |
| Na-rich electrolyte compositions provided herein can be used in a variety of devices, such as sodium ionic batteries, capacitors and other electrochemical devices. Na-rich electrolyte compositions provided herein can have a chemical formula of Na3OX, Na3SX, Na (3-δ) Mδ/2OX and Na (3-δ) Mδ/2SX wherein 0<δ<0.8, wherein X is a monovalent anion selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof, and wherein M is a divalent metal selected from the group consisting of magnesium, calcium, barium, strontium and mixtures thereof. Na-rich electrolyte compositions provided herein can have a chemical formula of Na (3-δ) Mδ/3OX and/or Na (3-δ) Mδ/3SX; wherein 0<δ<0.5, wherein M is a trivalent cation M3, and wherein X is selected from fluoride, chloride, bromide, iodide, H−, CN−, BF4−, BH4−, ClO4−, CH3−, NO2−, NH2− and mixtures thereof. Synthesis and processing methods of NaRAP compositions for battery, capacitor, and other electrochemical applications are also provided. | ||||||
| 75 | FLUORINATING AGENT | US15026349 | 2014-10-02 | US20160332877A1 | 2016-11-17 | Shoji HARA; Yosuke KISHIKAWA; Atsushi SHIRAI; Takashi NAMIKAWA; Sumi ISHIHARA |
| An object of the present invention is to provide a novel substance that has a high reactivity as a fluorinating agent, is effectively used in various fluorination reactions, and is safely handled even in air. As the solution for achieving this object, the present invention provides a complex obtained by reacting bromine trifluoride with at least one metal halide selected from the group consisting of halogenated metals and halogenated hydrogen metals in a nonpolar solvent. This complex serves as a fluorinating agent that provides excellent fluorination performance and that is stable in air. | ||||||
| 76 | Titanate and titania nanostructures and nanostructure assemblies, and methods of making same | US13872867 | 2013-04-29 | US09365432B2 | 2016-06-14 | Stanislaus S. Wong; Yuanbing Mao |
| The invention relates to nanomaterials and assemblies including, a micrometer-scale spherical aggregate comprising: a plurality of one-dimensional nanostructures comprising titanium and oxygen, wherein the one-dimensional nanostructures radiate from a hollow central core thereby forming a spherical aggregate. | ||||||
| 77 | Method for producing imide salt | US14352175 | 2012-09-25 | US09352966B2 | 2016-05-31 | Atsushi Fukunaga; Shinji Inazawa; Koji Nitta; Shoichiro Sakai |
| A mixture of sulphamic acid, a halogenated sulphonic acid and thionyl chloride is heated to allow the reaction to proceed, to thereby produce first intermediate products. The first intermediate products are then subjected to reaction with an alkali metal fluoride MF to produce second intermediate products. The second intermediate products is then subjected to reaction with the alkali metal fluoride MF in a polar solvent to obtain a desired product MN(SO2F)2 (where M is an alkali metal). | ||||||
| 78 | Boride having chemical composition Na—Si—B, and polycrystalline reaction sintered product of boride and process for production thereof | US13817646 | 2011-08-17 | US09255010B2 | 2016-02-09 | Haruhiko Morito; Hisanori Yamane |
| Provided are: a novel bonds useful as a highly-functional material; and a novel production method for a polycrystalline sintered product of a bonds, of which the energy cost is low, which does not require a sintering promoter, which enables the product to be worked into complicated forms and which enables a development to a polynary boride.Provided are a boride having a composition Na—Si—B, and a polycrystalline reaction-sintered product thereof. A mixed compact of boron and an element, M (M means Si and/or C) is heated along with metal sodium to give a polycrystalline reaction-sintered product. | ||||||
| 79 | TITANATE AND TITANIA NANOSTRUCTURES AND NANOSTRUCTURE ASSEMBLIES, AND METHODS OF MAKING SAME | US13872867 | 2013-04-29 | US20150239748A1 | 2015-08-27 | Stanislaus S. Wong; Yuanbing Mao |
| The invention relates to nanomaterials and assemblies including, a micrometer-scale spherical aggregate comprising: a plurality of one-dimensional nanostructures comprising titanium and oxygen, wherein the one-dimensional nanostructures radiate from a hollow central core thereby forming a spherical aggregate. | ||||||
| 80 | Process for production hexafluorophosphates | US12993175 | 2009-08-04 | US09059480B2 | 2015-06-16 | Masahide Waki; Tatsuhiro Yabune; Kazuhiro Miyamoto; Kazutaka Hirano |
| An object is to provide a method of manufacturing a hexafluorophosphate, that can simply and easily manufacture an inexpensive and high-quality hexafluorophosphate while suppressing the manufacturing cost, an electrolytic solution containing a hexafluorophosphate, and an electricity storage device including the electrolytic solution. The present invention relates to a method of manufacturing a hexafluorophosphate, which comprises reacting at least a phosphorus compound with a fluoride represented by MFs.r(HF) (wherein 0≦r≦6, 1≦s≦3, and M is at least one kind selected from the group consisting of Li, Na, K, Rb, Cs, NH4, Ag, Mg, Ca, Ba, Zn, Cu, Pb, Al and Fe) to produce a hexafluorophosphate represented by the chemical formula M(PF6)s. | ||||||
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