序号 专利名 申请号 申请日 公开(公告)号 公开(公告)日 发明人
1 一种硝酸的制备方法 CN201610598895.2 2016-07-22 CN106276985A 2017-01-04 孙进贺; 贾永忠; 张全有; 景燕; 谢绍雷; 马贵香
发明公开了一种硝酸的制备方法,包括步骤:A、将硝酸盐与性共熔助剂混合均匀并加热至不超过300℃,进行熔融,获得第一混合物;其中,硝酸盐与碱性共熔助剂的质量之比不小于3:1;B、将富钾岩石粉碎并置于第一混合物中,继续加热至不超过600℃,并保温6h~24h,获得第二混合物;其中,富钾岩石是指以K2O计时其质量百分数不低于8%的酸盐矿物;C、将第二混合物冷却至100℃~120℃后通入,获得第三混合物,使第三混合物在50℃~90℃下保温6h~36h,固液分离,获得第一滤渣和第一滤液;D、第一滤液经浓缩、冷却,析出硝酸钾。根据本发明的硝酸钾的制备方法,其以富钾岩石为原料,通过两次浸取即可获得硝酸钾水溶液,工艺简单、能耗低、且绿色环保。
2 一种硝酸的制备方法 CN201610584010.3 2016-07-22 CN106276984A 2017-01-04 孙进贺; 贾永忠; 张全有; 景燕; 谢绍雷; 姚颖
发明公开了一种硝酸的制备方法,包括步骤:A、将硝酸盐加热至不超过300℃,进行熔融,获得第一熔融物;B、将富钾岩石粉碎并置于所述第一熔融物中,继续加热至不超过600℃,并保温12h~36h,获得第二熔融物;其中,所述富钾岩石是指以K2O计时K2O的质量百分数不低于8%的酸盐矿物;C、将所述第二熔融物冷却至100℃~120℃后向其中通入,获得混合体系,使所述混合体系在50℃~90℃下保温6h~48h,固液分离,获得第一滤渣和第一滤液;D、所述第一滤液经浓缩、冷却,析出硝酸钾。根据本发明的硝酸钾的制备方法,其以富钾岩石为原料,通过两次浸取即可获得硝酸钾水溶液,工艺简单、能耗低、且绿色环保。
3 Method and process for the leaching of caliche and for the recovery of nitrate therefrom US51333521 1921-11-07 US1517046A 1924-11-25 LALOR BURDICK CHARLES
4 Purification or extraction of soluble substances US56804622 1922-06-13 US1439061A 1922-12-19 WALTER BROADBRIDGE; EDWIN EDSER; GEORGE SELLERS WILLIAM
5 Process of treating alkali-metal-salt mixtures US28529919 1919-03-26 US1363092A 1920-12-21 CULLEN JOHN A
6 Process of extracting potassium from minerals. US20544717 1917-12-04 US1296458A 1919-03-04 BLUMENBERG HENRY JR
7 Method of purifying alkaline cyanids. US1901068409 1901-07-15 US684914A 1901-10-22 CRAIG GEORGE
8 Control of percolation leaching of ores exhibiting a significant heat of solution US34712364 1964-02-25 US3334973A 1967-08-08 GOREN MAYER B; MEYER ADOLPH E
9 Treatment of nitrate-bearing material US70440933 1933-12-29 US2040548A 1936-05-12 STANLEY FREED EDGAR
10 Treatment of crude mineral salts US24134727 1927-12-20 US1813575A 1931-07-07 ERNST JANECKE; HERMANN KLIPPEL; EMIL HEGELMANN
11 Production of sodium nitrate US22139427 1927-09-22 US1696197A 1928-12-25 ROBERT GRIESSBACH; KURT ROHRE
12 Process of leaching and obtaining nitrates and chlorids US15765117 1917-03-27 US1357973A 1920-11-09 GIESECKE WILLIAM E
13 Harry p US1194465D US1194465A 1916-08-15
14 A PROCESS FOR PRODUCING HIGH-PURITY POTASSIUM SALTS EP97926033.8 1997-06-12 EP0904251B1 2001-09-19 VORAGE, Marcus; EICHNER, Per
The present invention relates to a new selective process for producing high-purity potassium nitrate or potassium phosphate. The process uses a liquid agricultural or fermentation by-product, such as molasses, vinasse or potato thick juice as its potassium source and comprises the following unit operations: clarification, ion exchange, neutralization, concentration and crystallization. Importantly, the present invention also concerns a process for producing an ingredient for animal feed, said ingredient having a reduced potassium content.
15 A PROCESS FOR PRODUCING HIGH-PURITY POTASSIUM SALTS EP97926033.0 1997-06-12 EP0904251A1 1999-03-31 VORAGE, Marcus; EICHNER, Per
The present invention relates to a new selective process for producing high-purity potassium nitrate or potassium phosphate. The process uses a liquid agricultural or fermentation by-product, such as molasses, vinasse or potato thick juice as its potassium source and comprises the following unit operations: clarification, ion exchange, neutralization, concentration and crystallization. Importantly, the present invention also concerns a process for producing an ingredient for animal feed, said ingredient having a reduced potassium content.
16 Process for producing high-purity potassium salts US09194903 1998-12-04 US06274105B1 2001-08-14 Marcus Vorage; Per Eichner
The present invention relates to a new selective process for producing high-purity potassium nitrate or potassium phosphate. The process uses a liquid agricultural or fermentation by-product, such as molasses, vinasse or potato thick juice as its potassium source and comprises the following unit operations: clarification, ion exchange, neutralization, concentration and crystallization. Importantly, the present invention also concerns a process for producing an ingredient for animal feed, said ingredient having a reduced potassium content.
17 Process for the production of clear leach liquors US7123625 1925-11-24 US1731450A 1929-10-15 ALLEN ARTHUR W
18 Purification or extraction of soluble substances US56804722 1922-06-13 US1562863A 1925-11-24 WALTER BROADBRIDGE; EDWIN EDSER; GEORGE SELLERS WILLIAM
19 Manufacture of sodium nitrate US53043722 1922-01-19 US1516550A 1924-11-25 CAPPELEN SMITH ELIAS ANTHON
20 Recovery of nitrate from caliche US50832421 1921-10-17 US1513014A 1924-10-28 CAPPELEN SMITH ELIAS ANTHON
QQ群二维码
意见反馈