| 序号 | 专利名 | 申请号 | 申请日 | 公开（公告）号 | 公开（公告）日 | 发明人 |
|---|---|---|---|---|---|---|
| 21 | Milling process | US12158258 | 2006-12-19 | US07909272B2 | 2011-03-22 | Marc Thijssen; Maxime Franc |
| Process for milling a substance selected from sodium carbonate, sodium bicarbonate and sodium sesquicarbonate or trona, in which a cleaning agent is introduced into a mill for the purpose of obtaining a powder with a mean diameter of less than 100 μm and of inhibiting the formation of incrustations in the mill. | ||||||
| 22 | HIGH PURITY SODIUM HYDROGENCARBONATE CRYSTAL PARTICLES AND PROCESS FOR PRODUCING THE SAME | US12209253 | 2008-09-12 | US20090016949A1 | 2009-01-15 | Hachirou Hirano; Takako Hirano; Hisakazu Arima; Shintaro Kikuchi; Fumiaki Nakashima; Shigeru Sakurai |
| Sodium hydrogencarbonate crystal particles excellent in anti-caking property and anti-thermal decomposition property, and its production process, are provided.Sodium hydrogencarbonate crystal particles whose color 1 second after dropping of a phenolphthalein solution having a predetermined composition, is R=245 to 255, G=243 to 255 and B=245 to 255 in RGB 256 tone notation. The sodium hydrogencarbonate crystal particles are produced by subjecting sodium hydrogencarbonate crystal particles to a bicarbonation treatment in a humidified carbon dioxide gas atmosphere. | ||||||
| 23 | METHOD FOR EVALUATING CAKING PROPERTY OF SODIUM HYDROGENCARBONATE CRYSTAL PARTICLES | US11619286 | 2007-01-03 | US20070105226A1 | 2007-05-10 | Hachirou HIRANO; Takako Hirano; Shintaro Kikuchi; Fumiaki Nakashima; Hisakazu Arima; Shigeru Sakurai |
| A method for evaluating the caking property of sodium hydrogencarbonate crystal particles, characterized in that sodium hydrogencarbonate crystal particles are hermetically sealed in a packaging material having a water vapor transmission rate of at least 3 g/(m2·24h) (at 40° C. with a relative humidity difference of 90%) as stipulated in JIS K7129 and left at rest at a temperature of from 17 to 35° C. at a carbon dioxide gas concentration of from 0.03 to 0.05 vol % at a relative humidity of from 40 to 95% for from 2 weeks to 3 months, and the proportion of agglomerated sodium hydrogencarbonate crystal particles is determined to evaluate the caking tendency. A novel test method for evaluating the caking property of sodium hydrogencarbonate crystal particles, capable of providing results of the caking property test with high reproducibility, quantitatively with high versatility, can be provided. | ||||||
| 24 | Free-flowing potassium bicarbonate composition | US558411 | 1995-11-16 | US5552084A | 1996-09-03 | M. Stephen Lajoie; Robin C. Sargent |
| This invention provides a process for producing a particulate potassium bicarbonate composition which maintains its free-flow properties when stored under ambient temperature and relative humidity conditions. In the process, particulate potassium bicarbonate is blended with fine grain alkaline earth metal oxide, and the oxide is microdispersed on the surface of the particles. The oxide reacts with moisture and carbon dioxide to form an adherent physically-bonded coating of alkaline earth metal carbonate on the surface of the potassium bicarbonate particles. The altered particle surface prevents agglomeration of the potassium bicarbonate particles. | ||||||
| 25 | Methods for production of alkali metal polysilicates | US19347171 | 1971-10-28 | US3835216A | 1974-09-10 | ALMAGRO G; BERTORELLI O; ZIMMERMAN H; MAYS R; WILLIAMS L |
| A method for producing alkali metal polysilicates is disclosed. Polysilicates, produced by hydrothermally reacting an aqueous dispersion of finely divided silica and an alkali metal hydroxide are spray dried and the solid product is fractured and pulverized. The fractured mass is then pelletized employing the solubility of the polysilicates to form a free-flowing product having a continuous, even surface. Pelletization may be effected with or without the use of water and/or binders.
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| 26 | Process and apparatus for storage and recovery of soluble materials | US67899933 | 1933-07-03 | US2043710A | 1936-06-09 | WALTER ROWLAND |
| 27 | 밀링 방법 | KR1020087017845 | 2006-12-19 | KR1020080081181A | 2008-09-08 | 티센마르끄; 프랑맥심 |
| Process for milling a substance selected from sodium carbonate, sodium bicarbonate and sodium sesquicarbonate or trona, in which a cleaning agent is introduced into a mill for the purpose of obtaining a powder with a mean diameter of less than 100 mum and of inhibiting the formation of incrustations in the mill. | ||||||
| 28 | 酸性成分除去剤の製造方法および気体中の酸性成分除去方法 | JP2012533947 | 2011-09-05 | JPWO2012036012A1 | 2014-02-03 | 桜井 茂; 茂 桜井; 高田 英樹; 英樹 高田; 松本 知子; 知子 松本 |
| バグフィルタの濾布における圧力損失の上昇、濾布からの酸性成分除去剤の漏れを抑制し、サイロからの排出トラブルが発生しにくく、取り扱い性に優れ、濾布の表面に堆積した濾過層の脱落を充分に抑制できる酸性成分除去剤の製造方法を提供する。平均粒子径が50μm以上の炭酸水素ナトリウム(A)の粉体と、疎水性ヒュームドシリカ(B)の粉体と、1次粒子の平均粒子径が50nm以下の膠質炭酸カルシウム(C)の粉体とを混合し粉砕して酸性成分除去剤の粉体を製造する方法であり、得られる酸性成分除去剤の平均粒子径を3〜20μm、酸性成分除去剤中の前記疎水性ヒュームドシリカ(B)の含有割合を0.2〜0.5質量%、および、酸性成分除去剤中の前記膠質炭酸カルシウム(C)の含有割合を1.5〜2.5質量%、とする。 | ||||||
| 29 | Caking evaluation method of sodium hydrogen carbonate crystal particles | JP2006528819 | 2005-06-30 | JP4826473B2 | 2011-11-30 | 史暁 中島; 八朗 平野; 寿一 有馬; 茂 桜井; 真太郎 菊地 |
| 30 | Method for producing sodium hydrogencarbonate crystal particle having low caking property | JP2010049663 | 2010-03-05 | JP2010159208A | 2010-07-22 | HIRANO HACHIRO; YOKOYAMA KOICHI; YAMAMOTO KIYOSHI; NARIZUKA TEIJI |
| PROBLEM TO BE SOLVED: To provide a method for producing and packaging sodium hydrogencarbonate (baking soda) crystal particles having a low caking property, which do not need the addition of a caking inhibitor thereto and are suitable for use in the fields of food, pharmaceuticals and bath agents. SOLUTION: Sodium hydrogencarbonate crystal particles having a mean particle diameter of 50-500 μm are produced by deposition from mother liquor of an aqueous solution containing sodium hydrogencarbonate having potassium concentration of ≤400 mass ppm, and the sodium hydrogencarbonate crystal particles are dried using a dry gas having carbon dioxide concentration of ≥3 vol.% to produce sodium hydrogencarbonate crystal particles having potassium concentration of ≤50 mass ppm and carbonate ion concentration of ≤1 mass% in terms of sodium carbonate. COPYRIGHT: (C)2010,JPO&INPIT | ||||||
| 31 | 炭酸水素ナトリウム結晶粒子の固結性評価方法 | JP2006528819 | 2005-06-30 | JPWO2006004004A1 | 2008-04-17 | 平野 八朗; 八朗 平野; 真太郎 菊地; 史暁 中島; 寿一 有馬; 桜井 茂; 茂 桜井 |
| 炭酸水素ナトリウム結晶粒子を、JIS K 7129で規定される水蒸気透過度(40℃、相対湿度差90%)として3g/(m2・24h)以上を有する包装材料で密閉して、温度が17〜35℃、二酸化炭素ガス濃度が0.03〜0.05容量%、かつ40〜95%の間の相対湿度で2週間〜3月間静置し、塊状となった炭酸水素ナトリウム結晶粒子の割合を求めることにより固結のしやすさを評価することを特徴とする炭酸水素ナトリウムの固結性評価方法。再現性が良く、定量的で、汎用性の高い、固結試験の結果を得ることができる、炭酸水素ナトリウム結晶粒子の新規な固結評価試験方法を提供できる。 | ||||||
| 32 | Manufacturing method for sodium hydrogencarbonate crystal particle with low caking property, and sodium hydrogencarbonate crystal | JP2003091444 | 2003-03-28 | JP2004002166A | 2004-01-08 | HIRANO HACHIRO; YOKOYAMA KOICHI; YAMAMOTO KIYOSHI; NARIZUKA TEIJI |
| PROBLEM TO BE SOLVED: To provide a manufacturing method and a wrapping method for sodium hydrogencarbonate (sodium bicarbonate) crystal particles having low caking properties, needing no addition of an anticaking agent, and suitable for the fields of food, medicines, and bath salts. SOLUTION: The potassium concentration in sodium hydrogencarbonate crystals with an average particle size of 50-500 μm is lowered to 50 mass ppm or lower, preferably to as low as possible, and the carbonate ion concentration (in terms of sodium carbonate) in the crystal particles is lowered to 1 mass% or lower. Such crystal particles can be obtained by washing sodium hydrogencarbonate crystals with water or an aqueous sodium hydrogencarbonate solution and drying or can be obtained by lowering the potassium concentration in a mother liquor to 400 mass ppm or lower in manufacturing the sodium hydrogencarbonate crystal particles by causing the particles to settle from the mother liquor. Thus obtained sodium hydrogencarbonate is sealed with a wrapping material with a moisture permeability (according to JIS Z0208) at 40°C of 5 g/m 2/day or lower. COPYRIGHT: (C)2004,JPO | ||||||
| 33 | How to clean the gas of the acidic compounds | JP2000530045 | 1999-01-21 | JP2002501823A | 2002-01-22 | ニコラ アーヴェランジュ; メーディー ゴードシ; ポール デミリー; レオン ニナーヌ; ステファン ポーラエル |
| (57)【要約】 ２m 2 /gより高い比表面積を有し、その取扱中、相対湿度が２０％未満の大気中に保持する及び／または乾燥剤を混合する、無水炭酸ナトリウム粉末を含む塩基性試薬で気体を乾式または半湿式処理する方法で酸性化合物の気体を精製する方法。 | ||||||
| 34 | Alkali metal bicarbonate particles with exceptional flowability | EP14199912.8 | 2014-12-22 | EP3037387A1 | 2016-06-29 | SAVARY, David Jean Lucien |
The invention leads to powder compositions comprising alkali metal bicarbonate particles and an amino acid as additive. The invention also relates to a process for preparing alkali metal bicarbonate particles by spray-drying of an aqueous solution comprising 1 - 10 % by weight of alkali metal bicarbonate and an amino acid as additive. |
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| 35 | PROCESS FOR PRODUCING SODIUM HYDROGEN CARBONATE CRYSTAL GRAIN OF LOW CAKING TENDENCY | EP05765277.8 | 2005-06-30 | EP1770066B1 | 2016-04-27 | HIRANO, Hachirou, c/o Asahi Glass Company, Limited; KIKUCHI, Shintaro, c/o Asahi Glass Company, Limited; NAKASHIMA, Fumiaki, c/o Asahi Glass Company, Limited; ARIMA, Hisakazu, c/o Asahi Glass Company, Limited; SAKURAI, Shigeru, c/o Asahi Glass Company, Limited |
| 36 | MILLING PROCESS | EP06841440.8 | 2006-12-19 | EP1966087B1 | 2015-07-08 | THIJSSEN, Marc; FRANC, Maxime |
| 37 | SODIUM HYDROGENCARBONATE CRYSTAL GRAINS WITH LOW LEVEL OF INTEGRITY AND PROCESS FOR PRODUCING THE SAME | EP05765181 | 2005-06-30 | EP1770065A4 | 2011-02-23 | HIRANO HACHIROU; KIKUCHI SHINTARO; NAKASHIMA FUMIAKI; ARIMA HISAKAZU; SAKURAI SHIGERU |
| 38 | Method for producing sodium hydrogencarbonate crystal particles having a low caking property, and sodium hydrogencarbonate crystal particles | EP03006843.1 | 2003-03-27 | EP1357085B1 | 2006-09-27 | Yokoyama, Kouichi, Asahi Glass Company, Limited; Narituka, Sadaji, Asahi Glass Company, Limited; Yamamoto, Kiyoshi, Asahi Glass Company, Limited; Hirano, Hachiro, Asahi Glass Company, Limited |
| 39 | Method for producing sodium hydrogencarbonate crystal particles having a low caking property, and sodium hydrogencarbonate crystal particles | EP03006843.1 | 2003-03-27 | EP1357085A2 | 2003-10-29 | Yokoyama, Kouichi, Asahi Glass Company, Limited; Narituka, Sadaji, Asahi Glass Company, Limited; Yamamoto, Kiyoshi, Asahi Glass Company, Limited; Hirano, Hachiro, Asahi Glass Company, Limited |
A method for producing sodium hydrogencarbonate crystal particles having a low caking property, which comprises lowering the potassium concentration in sodium hydrogencarbonate crystal particles having a mean particle diameter of from 50 to 500 µm to a level of at most 50 mass ppm. |
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| 40 | 非常に優れた流動性を有するアルカリ金属重炭酸塩粒子 | JP2017533425 | 2015-12-22 | JP2018502814A | 2018-02-01 | サヴァリー, ダヴィド ジャン リュシアン |
| 本発明は、アルカリ金属重炭酸塩粒子と、添加剤としてのアミノ酸とを含有する粉末組成物をもたらす。本発明は、1〜10重量%のアルカリ金属重炭酸塩と、添加剤としてのアミノ酸とを含む水溶液を噴霧乾燥することによる、アルカリ金属重炭酸塩粒子の作製方法にも関する。本発明は更に、添加剤としてのアミノ酸の存在下でアルカリ金属重炭酸塩を共粉砕することによる、アルカリ金属重炭酸塩粒子の作製方法にも関する。【選択図】なし | ||||||
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