首页 / 专利分类库 / 有机化学 / 无环或碳环化合物 / 硫醇、硫醚、氢化多硫化物或多硫化物的制备 / Preparation of oil solution containing alkaline earth metal salt of alkylphenol sulfide with high basicity

Preparation of oil solution containing alkaline earth metal salt of alkylphenol sulfide with high basicity

专利类型 发明专利 法律事件
专利有效性 失效专利 当前状态
申请号 JP10577083 申请日 1983-06-15
公开(公告)号 JPS59232189A 公开(公告)日 1984-12-26
申请人 Taiyo Kako Kk; 申请人类型 企业
发明人 MURAKAMI MITSUHIRO; MIKAMI TAKUHIRO; SUZUKI AKITO; 第一发明人 MURAKAMI MITSUHIRO
权利人 Taiyo Kako Kk 权利人类型 企业
当前权利人 Taiyo Kako Kk 当前权利人类型 企业
省份 当前专利权人所在省份: 城市 当前专利权人所在城市:
具体地址 当前专利权人所在详细地址: 邮编 当前专利权人邮编:
主IPC国际分类 C10M159/22 所有IPC国际分类 C10M159/22C07C67/00C07C313/00C07C319/00C07C323/18C07C323/20C10N30/04C10N40/25C10M1/38C07C149/30
专利引用数量 0 专利被引用数量 1
专利权利要求数量 0 专利文献类型 A
专利代理机构 专利代理人
摘要 PURPOSE:To prepare the titled oil soln. having a low viscocity and excellent oil solubility in a simple operation, by using a weakly acidic metal salt as catalyst in the reaction of alkylphenol with elemental sulfur to produce an alkylphenol sulfide. CONSTITUTION:Alkylphenol having an 8-22C alkyl group (e.g. nonylphenol) is made to react with elemental sulfur in the presence of a weakly acidic metal salt catalyst (e.g. sodium acetate) and then a monohydric alcohol (e.g. tridecanol), a lubricating oil medium, a (hydr)oxide of an alkaline earth metal (e.g. calcium hydroxide) and a dihydric alcohol (e.g. ethylene glycol) are added to the reaction product. Carbon dioxide gas is blown into the resultant mixture for saturation and volatile components are removed from the reaction product by distillation to obtain the oil soln.
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