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Carboxylation of grignard reagents in the presence of liquid co2

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1. THE METHOD OF PREPARING A CARBOXYLATED GRIGNARD REAGENT WHICH COMPRISES REACTING SAID GRIGNARD REAGENT WITH CARBON DIOXIDE IN A REACTION MIXTURES; MAINTAINING A BODY OF LIQUID CARBON DIOXIDE IN CONTACT WITH SAID REACTION MIXTURE DURING SAID REACTION; VOLATILIZING CARBON DIOXIDE FROM SAID BODY OF LIQUID CARBON DIOXIDE INTO SAID REACTION MIXTURE THEREBY EXTRACTING HEAT FROM SAID REACTION MIXTURE AND MAINTAINING SAID REACTION MIXTURE AT CONTROLLED TEMPERATURE; AND WITHDRAWING PRODUCT CARBOXYLATED GRIGNARD REAGENT FROM SAID REACTION MIXTURE.
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