序号 专利名 申请号 申请日 公开(公告)号 公开(公告)日 发明人
1 流体处理方法 CN201480024365.6 2014-04-28 CN105246585B 2017-05-03 榎村真一
发明提供一种有效地控制被处理流动体的处理特性的流体处理方法。具备可接近·分离的、相对旋转的处理用面(1、2),使被处理流动体从内侧向外侧穿过处理用面(1、2)间的处理区域作为薄膜流体,进行成为所述薄膜流体的被处理流动体的处理。通过使从旋转的中心到外周端的距离(Od)相对于从旋转的中心到中间导入部d2的距离(Cd)的比例(Od/Cd)变化,来控制处理特性。
2 结晶系统和方法 CN201380079070.4 2013-06-24 CN105592901A 2016-05-18 沃尔夫冈·赫恩佐
用于使溶解在溶剂中的要被结晶出来的物质结晶的系统,所述系统具有结晶装置,要被浓缩的溶液,以及加热蒸汽或加热液体流过所述结晶装置,所述溶液包括具有在其中溶解的要被结晶出来的所述物质的所述溶剂,其中所述结晶装置具有携带所述要被浓缩的溶液的至少一个流通道、携带所述加热蒸汽或加热液体的至少一个流通道、和携带蒸汽状溶剂的至少一个流通道,其中通过蒸汽不可渗透和液体不可渗透的壁,携带所述要被浓缩的溶液的相应流通道与携带所述加热蒸汽或加热液体的相应流通道至少部分隔离,以及通过对蒸汽状溶剂可渗透但对液体溶剂不可渗透的膜壁,携带所述要被浓缩的溶液的相应流通道与携带所述蒸汽状溶剂的相应流通道至少部分隔离,其中所述结晶装置设计使得所述要被浓缩的溶液在携带所述要被浓缩的溶液的所述相应流通道中沉积以及在沉积过程中产生的所述蒸汽状溶剂通过所述膜壁到携带所述蒸汽状溶剂的邻近流通道中。
3 微粒的制造方法 CN201280070893.6 2012-02-29 CN104136110B 2017-03-08 榎村真一
发明的课题在于提供微粒的制造方法。提供微粒的制造方法。作为第1工序,在对向配设了的、可接近·分离的、至少一方相对于另一方相对进行旋转的至少2个处理用面之间形成的薄膜流体中,使晶种微粒析出,将含有析出了的晶种微粒的流体作为排放液而排出。之后,作为第2工序,在排出了的排放液中,使析出的晶种微粒成长而得到目标微粒。在微粒的制造方法中,通过含有上述的2个工序,得到均匀且均质的微粒。
4 流体处理方法 CN201480024365.6 2014-04-28 CN105246585A 2016-01-13 榎村真一
发明提供一种有效地控制被处理流动体的处理特性的流体处理方法。具备可接近·分离的、相对旋转的处理用面(1、2),使被处理流动体从内侧向外侧穿过处理用面(1、2)间的处理区域作为薄膜流体,进行成为所述薄膜流体的被处理流动体的处理。通过使从旋转的中心到外周端的距离(Od)相对于从旋转的中心到中间导入部d2的距离(Cd)的比例(Od/Cd)变化,来控制处理特性。
5 一种分级结晶物质的方法,适用于该方法的结晶器,以及该方法的用途 CN98115497.2 1998-07-16 CN1103621C 2003-03-26 M·斯特潘斯基; B·J·杨斯
在本发明的分级结晶当被结晶时对结晶器的基本上垂直的结晶表面(39)具有较弱的附着的物质,特别是石蜡、油、脂肪和蜡的方法中,将例如由弯曲成锯齿形的多孔金属板(3 1)制成的网状支承结构设置在结晶器的结晶表面(39)之间。在进行热析相期间从结晶表面(39)脱落的结晶(51)被悬置于多孔板(31)上的三区(41)区中的平条上并与结晶表面(39)保持热接触和热析出液相(55)。母液(55)向下滴淌,并且在某些场合下还在结晶(51)和结晶表面(39)之间滴淌,结果下降的通道被热的母液所熔化并因此而被打开。
6 结晶系统和方法 CN201480011699.X 2014-01-09 CN105142748B 2017-07-25 沃尔夫冈·赫恩佐
发明涉及一种用于溶剂中溶解和待结晶材料的结晶的系统,其具有由待浓缩溶液和液体流动通过的结晶设备,所述溶液具有溶剂以及其中的所述溶解和待结晶材料,所述液体与所述待浓缩溶液相比具有较低温度,其中所述结晶设备具有至少一个用于引导所述待浓缩溶液的流道并且具有至少一个用于引导所述液体的流道,其中用于引导所述待浓缩溶液的各别流道的内部空间至少部分由可被蒸气类溶剂但不可被液体溶剂渗透的薄膜壁结合,并且用于引导所述液体的各别流道靠近至少一个用于引导所述待浓缩溶液的各别流道,由此通过所述薄膜壁以使得所述溶剂从所述待浓缩溶液通过所述薄膜壁的方式设定蒸气压差。
7 结晶系统和方法 CN201480011699.X 2014-01-09 CN105142748A 2015-12-09 沃尔夫冈·赫恩佐
发明涉及一种用于溶剂中溶解和待结晶材料的结晶的系统,其具有由待浓缩溶液和液体流动通过的结晶设备,所述溶液具有溶剂以及其中的所述溶解和待结晶材料,所述液体与所述待浓缩溶液相比具有较低温度,其中所述结晶设备具有至少一个用于引导所述待浓缩溶液的流道并且具有至少一个用于引导所述液体的流道,其中用于引导所述待浓缩溶液的各别流道的内部空间至少部分由可被蒸气类溶剂但不可被液体溶剂渗透的薄膜壁结合,并且用于引导所述液体的各别流道靠近至少一个用于引导所述待浓缩溶液的各别流道,由此通过所述薄膜壁以使得所述溶剂从所述待浓缩溶液通过所述薄膜壁的方式设定蒸气压差。
8 微粒的制造方法 CN201280070893.6 2012-02-29 CN104136110A 2014-11-05 榎村真一
发明的课题在于提供微粒的制造方法。提供微粒的制造方法。作为第1工序,在对向配设了的、可接近·分离的、至少一方相对于另一方相对进行旋转的至少2个处理用面之间形成的薄膜流体中,使晶种微粒析出,将含有析出了的晶种微粒的流体作为排放液而排出。之后,作为第2工序,在排出了的排放液中,使析出的晶种微粒成长而得到目标微粒。在微粒的制造方法中,通过含有上述的2个工序,得到均匀且均质的微粒。
9 一种分级结晶物质的方法,适用于该方法的结晶器,以及该方法的用途 CN98115497.2 1998-07-16 CN1209348A 1999-03-03 M·斯特潘斯基; B·J·杨斯
在本发明的分级结晶当被结晶时对结晶器的基本上垂直的结晶表面(39)具有较弱的附着的物质,特别是石蜡、油、脂肪和蜡的方法中,将例如由弯曲成锯齿形的多孔金属板(31)制成的网状支承结构设置在结晶器的结晶表面(39)之间。在进行热析相期间从结晶表面(39)脱落的结晶(51)被悬置于多孔板(31)上的三区(41)区中的平条上并与结晶表面(39)保持热接触和热析出液相(55)。母液(55)向下滴淌,并且在某些场合下还在结晶(51)和结晶表面(39)之间滴淌,结果下降的通道被热的母液所熔化并因此而被打开。
10 流体処理方法 JP2015514854 2014-04-28 JP6364593B2 2018-08-01 榎村 眞一
11 Process and apparatus for separating substances by crystallization US805325 1991-12-10 US5230769A 1993-07-27 Slobodan Jancic; Evangelos Sakellariou
A process is provided for the separation of substances by melt crystallization. The organic mixtures which are difficult to crystallize are heated to a temperature sufficient to obtain a melt with the melt then being moved through a three-dimensional crystallization matrix having a large specific area. The melt is slowly cooled over a temperature range so as to achieve a selective crystallization from the supersaturated melt in the carrier matrix. A deposited crystal phase is thereafter melted and separated from the carrier matrix and removed by centrifugation. The carrier matrix may have a crystallization-promoting microstructure surface and may consist of an openpored foam.
12 Process for fractional crystallization of substances, a crystallizer suitable for working the process, and use of the process US118701 1998-07-16 US6145340A 2000-11-14 Manfred Stepanski; Bernhard J. Jans
In the process according to the invention for fractionating substances, particularly paraffins, oils, fats and waxes, which, when crystallized, have poor adhesion to the substantially vertical crystallization surfaces (39) of a crystallizer, screen-like supporting structures, e.g. perforated metal sheets (31) bent in a zig-zag, are disposed between the crystallization surfaces (39) of a crystallizer. The crystals (51) becoming detached from the crystallization surfaces (39) during the sweating phase are left suspended in horizontal strips in the triangular zones (41) on the perforated sheet (31) and remain in thermal contact with the crystallization surface (39) and sweat out the liquid phase (55). The mother liquor (55) drips off, in some cases also between the crystals (51) and the crystallization surface (39), with the result that drip channels are melted by the heated mother liquor and thus opened.
13 流体処理方法 JP2015514854 2014-04-28 JPWO2014178387A1 2017-02-23 眞一 榎村
被処理流動体の処理特性を効率的に制御する流体処理方法を提供することを課題とする。接近・離反可能な、相対的に回転する処理用面1、2を備え、被処理流動体を、処理用面1、2間の処理領域に内側から外側に向けて通過せさて薄膜流体とし、前記薄膜流体となった被処理流動体の処理を行なう。回転の中心から中間導入部d2までの距離(Cd)に対する、回転の中心から外周端までの距離(Od)の割合(Od/Cd)を変化させることにより、処理特性を制御する。
14 微粒子の製造方法 JP2014501896 2012-02-29 JPWO2013128592A1 2015-07-30 榎村 眞一; 眞一 榎村
微粒子の製造方法を提供することを課題とする。微粒子の製造方法を提供する。第1の工程として、対向して配設された、接近・離反可能な、少なくとも一方が他方に対して相対的に回転する少なくとも2つの処理用面の間にできる薄膜流体中において、シード微粒子を析出させ、析出させたシード微粒子を含む流体を吐出液として排出させる。その後、第2の工程として、排出させた吐出液中において、析出させたシード微粒子を成長させて目的の微粒子を得る。微粒子の製造方法において、上記の2工程を含むことによって、均一かつ均質な微粒子を得る。
15 Crystallization method and crystallizer JP26636294 1994-10-04 JP2727061B2 1998-03-11 KIKUCHI KAZUO; UNNO HIROSHI; SHIBUYA HIROMITSU; MAKINO MASAHITO; SAKAKURA YASUYUKI; TAKAHASHI KYOSHI
Crystallization method and crystallization apparatus each use vertical plates for crystallization thereon. Both surfaces of the plate are used for different two liquids to flow down as films. Specifically, on one vertical surface, a feed liquid mixture containing crystallizable components therein flows down as a film, and on an opposite vertical surface, a cooling medium flows down as a film. Accordingly, the crystallizable component contained in the feed liquid mixture is cooled and crystallized to form crystal layers on the one vertical surface of the plate. The formed crystal layers are melted by a heating medium which flows down on the opposite vertical surface, and are collected as a melt. A pair of the plates may be used to form a unit to purify the liquid mixture on a large scale. A number of the units may be used to form a block which is suitable for a larger-scale crystallization processing. Further, a number of the blocks may be used to purify the liquid mixtures on a further larger-scale processing.
16 미립자의 제조 방법 KR1020147026084 2012-02-29 KR1020140138743A 2014-12-04 에노무라마사카즈
미립자의 제조 방법을 제공하는 것을 과제로 한다. 미립자의 제조 방법을 제공한다. 제 1 공정으로서 대향해서 배치되고, 접근·이반 가능하고, 적어도 한쪽이 다른쪽에 대하여 상대적으로 회전하는 적어도 2개의 처리용 면 사이에 생성되는 박막 유체 중에 있어서 시드 미립자를 석출시키고, 석출시킨 시드 미립자를 포함하는 유체를 토출액으로서 배출시킨다. 그 후, 제 2 공정으로서 배출시킨 토출액 중에 있어서 석출시킨 시드 미립자를 성장시켜서 목적의 미립자를 얻는다. 미립자의 제조 방법에 있어서 상기 2공정을 포함함으로써 균일하며 또한 균질한 미립자를 얻는다.
17 결정화 방법 및 장치 KR1019940026180 1994-10-13 KR100126611B1 1997-12-26 기꾸찌가즈오; 우미노요오; 시부따니히로미쯔; 마끼노마사히또; 사까꾸라야스유끼; 다까하시기요시
Crystallization method and crystallization apparatus each use vertical plates for crystallization thereon. Both surfaces of the plate are used for different two liquids to flow down as films. Specifically, on one vertical surface, a feed liquid mixture containing crystallizable components therein flows down as a film, and on an opposite vertical surface, a cooling medium flows down as a film. Accordingly, the crystallizable component contained in the feed liquid mixture is cooled and crystallized to form crystal layers on the one vertical surface of the plate. The formed crystal layers are melted by a heating medium which flows down on the opposite vertical surface, and are collected as a melt. A pair of the plates may be used to form a unit to purify the liquid mixture on a large scale. A number of the units may be used to form a block which is suitable for a larger-scale crystallization processing. Further, a number of the blocks may be used to purify the liquid mixtures on a further larger-scale processing.
18 Method and apparatus for growing crystals US71546 1998-05-01 US5997636A 1999-12-07 Moisey Y. Gamarnik; Ulises R. Alvarado
For growing crystals, either in ground testing or in space, a capillary tube is used, which contains the solution of the substance to be crystallized, a layer of absorbent and a layer of air or other gas separating the solution from the absorbent. Two absorbent layers may be used on opposite sides of the solution, each separated from the solution by a gaseous layer. To delay the onset of crystallization, the absorbent on each side may be separated from the solution by two gaseous layers, with a charge of absorbable liquid between them. An absorbent may be removed or modified by removing or perforating an end cap used to seal the absorbent within the capillary tube.
19 Method of and apparatus for crystallization US321995 1994-10-12 US5546763A 1996-08-20 Kazuo Kikuchi; Hiroshi Umino; Hiromitsu Shibuya; Masahito Makino; Yasuyuki Sakakura; Kiyoshi Takahashi
Crystallization method and crystallization apparatus each use vertical plates for crystallization thereon. Both surfaces of the plate are used for different two liquids to flow down as films. Specifically, on one vertical surface, a feed liquid mixture containing crystallizable components therein flows down as a film, and on an opposite vertical surface, a cooling medium flows down as a film. Accordingly, the crystallizable component contained in the feed liquid mixture is cooled and crystallized to form crystal layers on the one vertical surface of the plate. The formed crystal layers are melted by a heating medium which flows down on the opposite vertical surface, and are collected as a melt. A pair of the plates may be used to form a unit to purify the liquid mixture on a large scale. A number of the units may be used to form a block which is suitable for a larger-scale crystallization processing. Further, a number of the blocks may be used to purify the liquid mixtures on a further larger-scale processing.
20 Process and apparatus for separating substances by crystallization US36322 1993-03-24 US5338519A 1994-08-16 Slobodan Jancic; Evangelos Sakellariou
A process is provided for the separation of substances by melt crystallization. The organic mixtures which are difficult to crystallize are heated to a temperature sufficient to obtain a melt with the melt then being moved through a three-dimensional crystallization matrix having a large specific area. The melt is slowly cooled over a temperature range so as to achieve a selective crystallization from the supersaturated melt in the carrier matrix. A deposited crystal phase is thereafter melted and separated from the carrier matrix and removed by centrifugation. The carrier matrix may have a crystallization-promoting microstructure surface and may consist of an openpored foam.
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