专利名称:Microwave-assisted synthesis method for ruthenium (II) arene compound 收藏

Microwave-assisted synthesis method for ruthenium (II) arene compound
Microwave-assisted synthesis method for ruthenium (II) arene compound
申请号: CN201210338117.1 申请日: 2012-09-13
优先权号: CN201210338117 优先权日:
IPC分类号: C07F15/00
C07D471/14
主分类号: C07F15/00
申请人: UNIV GUANGDONG PHARM
专利权人:
发明人: WU QIONG
MEI WENJIE
第一发明人: WU QIONG
代理机构: 代理人:
摘要: The invention discloses a microwave-assisted synthesis method for a ruthenium (II) arene compound. The method comprises the following steps: adding a ruthenium (II) arene precursor, a phenanthrene imidazole derivative and dichloromethane to a reaction tube; introducing nitrogen into the microwave reaction tube; carrying out a microwave irradiation reaction at a temperature of 50 to 70 DEG G for 0.5 to 30 min; and after the reaction is finished, drying a reaction mixture through spinning, adding water for dissolution, carrying out filtration, drying mother liquor through spinning and carrying out re-crystallization. The microwave-assisted synthesis method for the ruthenium (II) arene compound provided by the invention has the advantages of high efficiency and high yield; compared with traditional heating methods, the method provided by the invention enables reaction time to be greatly shortened and reaction yield to be improved; and the method has a great application value in synthetic chemistry and industrial production.